Sub-second pair distribution function using a broad bandwidth monochromator Article Swipe
Nicolas P. L. Magnard
,
Daniel Risskov Sørensen
,
I. Kantor
,
Kirsten M. Ø. Jensen
,
Mads R. V. Jørgensen
·
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.1107/s1600576723004016
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.1107/s1600576723004016
Here the use of a broad energy bandwidth monochromator, i.e. a pair of B 4 C/W multilayer mirrors (MLMs), is demonstrated for X-ray total scattering (TS) measurements and pair distribution function (PDF) analysis. Data are collected both on powder samples and from metal oxo clusters in aqueous solution at various concentrations. A comparison between the MLM PDFs and those obtained using a standard Si(111) double-crystal monochromator shows that the measurements yield MLM PDFs of high quality which are suitable for structure refinement. Moreover, the effects of time resolution and concentration on the quality of the resulting PDFs of the metal oxo clusters are investigated. PDFs of heptamolybdate clusters and tungsten α-Keggin clusters from X-ray TS data were obtained with a time resolution down to 3 ms and still showed a similar level of Fourier ripples to PDFs obtained from 1 s measurements. This type of measurement could thus open up faster time-resolved TS and PDF studies.
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- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1107/s1600576723004016
- https://journals.iucr.org/j/issues/2023/03/00/vb5050/vb5050.pdf
- OA Status
- hybrid
- Cited By
- 2
- References
- 46
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4378909320
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- OpenAlex ID
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https://openalex.org/W4378909320Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.1107/s1600576723004016Digital Object Identifier
- Title
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Sub-second pair distribution function using a broad bandwidth monochromatorWork title
- Type
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articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2023Year of publication
- Publication date
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2023-05-17Full publication date if available
- Authors
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Nicolas P. L. Magnard, Daniel Risskov Sørensen, I. Kantor, Kirsten M. Ø. Jensen, Mads R. V. JørgensenList of authors in order
- Landing page
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https://doi.org/10.1107/s1600576723004016Publisher landing page
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https://journals.iucr.org/j/issues/2023/03/00/vb5050/vb5050.pdfDirect link to full text PDF
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YesWhether a free full text is available
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hybridOpen access status per OpenAlex
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https://journals.iucr.org/j/issues/2023/03/00/vb5050/vb5050.pdfDirect OA link when available
- Concepts
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Monochromator, Fourier transform, Pair distribution function, Materials science, Scattering, Tungsten, Molecular physics, Optics, Analytical Chemistry (journal), Chemistry, Physics, Wavelength, Chromatography, Quantum mechanics, MetallurgyTop concepts (fields/topics) attached by OpenAlex
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2Total citation count in OpenAlex
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2025: 1, 2023: 1Per-year citation counts (last 5 years)
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46Number of works referenced by this work
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10Other works algorithmically related by OpenAlex
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