Surface analysis by XRF and XPS for the Avogadro constant and the realization of the kilogram based on silicon spheres Article Swipe

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Edyta Beyer , Michael Kolbe , Matthias Müller , Erik Darlatt ·

YOU? · · 2017 · Open Access · · DOI: https://doi.org/10.24027/2306-7039.1a.2017.99448

The determination of the Avogadro constant for the redefinition of the SI unit kilogram as well as the eventual realization of the kilogram by monocrystalline enriched 28Si-spheres require a reliable surface analysis on silicon spheres. A novel instrumentation for the quantitative surface analysis of silicon spheres combines X-ray fluorescence spectroscopy and X-ray photoelectron spectroscopy techniques in order to enable the characterization and quantification of the oxide layer and unintentional contaminations. The analysis relies on the combination of the complementary X-ray methods. Measurements on 28Si-spheres were carried out. The surface was characterized regarding the elementary composition including the chemical binding states of the components and the mass of the surface layer

Related Topics

Avogadro Constant

X-Ray Photoelectron Spectroscopy

Kilogram

Silicon

Materials Science

Monocrystalline Silicon

Nuclear Magnetic Resonance

Concepts

Avogadro constant SPHERES X-ray photoelectron spectroscopy Kilogram Silicon Materials science Monocrystalline silicon Realization (probability) Characterization (materials science) Analytical Chemistry (journal) Surface (topology) Nanotechnology Physics Chemistry Thermodynamics Optoelectronics Chromatography Nuclear magnetic resonance Geometry Body weight Internal medicine Astronomy Medicine Mathematics Statistics

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Type: article
Language: en
Landing Page: https://doi.org/10.24027/2306-7039.1a.2017.99448
PDF: http://umj.metrology.kharkov.ua/article/download/99448/94581
OA Status: diamond
References: 3
Related Works: 10
OpenAlex ID: https://openalex.org/W2607586772

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DOI: https://doi.org/10.24027/2306-7039.1a.2017.99448

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Title: Surface analysis by XRF and XPS for the Avogadro constant and the realization of the kilogram based on silicon spheres

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Type: article

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Language: en

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Publication year: 2017

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Publication date: 2017-04-20

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Authors: Edyta Beyer, Michael Kolbe, Matthias Müller, Erik Darlatt

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Landing page: https://doi.org/10.24027/2306-7039.1a.2017.99448

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PDF URL: https://umj.metrology.kharkov.ua/article/download/99448/94581

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Concepts: Avogadro constant, SPHERES, X-ray photoelectron spectroscopy, Kilogram, Silicon, Materials science, Monocrystalline silicon, Realization (probability), Characterization (materials science), Analytical Chemistry (journal), Surface (topology), Nanotechnology, Physics, Chemistry, Thermodynamics, Optoelectronics, Chromatography, Nuclear magnetic resonance, Geometry, Body weight, Internal medicine, Astronomy, Medicine, Mathematics, Statistics

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referenced_works	https://openalex.org/W1994001382, https://openalex.org/W2045442593, https://openalex.org/W2123037222
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