Surface Studies on the Energy Release of the MOST System 2‐Carbethoxy‐3‐Phenyl‐Norbornadiene/Quadricyclane (PENBD/PEQC) on Pt(111) and Ni(111) Article Swipe
Felix Hemauer
,
Valentin Schwaab
,
Eva Marie Freiberger
,
Natalie J. Waleska‐Wellnhofer
,
Andreas Leng
,
Cornelius Weiß
,
Johann Steinhauer
,
Fabian Düll
,
Philipp Bachmann
,
Andreas Hirsch
,
Hans‐Peter Steinrück
,
Christian Papp
·
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.1002/chem.202203759
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.1002/chem.202203759
Novel energy‐storage solutions are necessary for the transition from fossil to renewable energy sources. Auspicious candidates are so‐called molecular solar thermal (MOST) systems. In our study, we investigate the surface chemistry of a derivatized norbornadiene/quadricyclane molecule pair. By using suitable push–pull substituents, a bathochromic shift of the absorption onset is achieved, allowing a greater overlap with the solar spectrum. Specifically, the adsorption and thermally induced reactions of 2‐carbethoxy‐3‐phenyl‐norbornadiene/quadricyclane are assessed on Pt(111) and Ni(111) as model catalyst surfaces by synchrotron radiation‐based X‐ray photoelectron spectroscopy (XPS). Comparison of the respective XP spectra enables the distinction of the energy‐rich molecule from its energy‐lean counterpart and allows qualitative information on the adsorption motifs to be derived. Monitoring the quantitative cycloreversion between 140 and 230 K spectroscopically demonstrates the release of the stored energy to be successfully triggered on Pt(111). Heating to above 300 K leads to fragmentation of the molecular framework. On Ni(111), no conversion of the energy‐rich compound takes place. The individual decomposition pathways of the two isomers begin at 160 and 180 K, respectively. Pronounced desorption of almost the entire surface coverage only occurs for the energy‐lean molecule on Ni(111) above 280 K; this suggests weakly bound species. The correlation between adsorption motif and desorption behavior is important for applications of MOST systems in heterogeneously catalyzed processes.
Related Topics
Concepts
Norbornadiene
Quadricyclane
Chemistry
X-ray photoelectron spectroscopy
Desorption
Photochemistry
Adsorption
Thermal desorption spectroscopy
Molecule
Thermal desorption
Cyanine
Catalysis
Crystallography
Physical chemistry
Organic chemistry
Physics
Nuclear magnetic resonance
Optics
Fluorescence
Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1002/chem.202203759
- https://onlinelibrary.wiley.com/doi/pdfdirect/10.1002/chem.202203759
- OA Status
- hybrid
- Cited By
- 4
- References
- 65
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4321996968
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W4321996968Canonical identifier for this work in OpenAlex
- DOI
-
https://doi.org/10.1002/chem.202203759Digital Object Identifier
- Title
-
Surface Studies on the Energy Release of the MOST System 2‐Carbethoxy‐3‐Phenyl‐Norbornadiene/Quadricyclane (PENBD/PEQC) on Pt(111) and Ni(111)Work title
- Type
-
articleOpenAlex work type
- Language
-
enPrimary language
- Publication year
-
2023Year of publication
- Publication date
-
2023-02-25Full publication date if available
- Authors
-
Felix Hemauer, Valentin Schwaab, Eva Marie Freiberger, Natalie J. Waleska‐Wellnhofer, Andreas Leng, Cornelius Weiß, Johann Steinhauer, Fabian Düll, Philipp Bachmann, Andreas Hirsch, Hans‐Peter Steinrück, Christian PappList of authors in order
- Landing page
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https://doi.org/10.1002/chem.202203759Publisher landing page
- PDF URL
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https://onlinelibrary.wiley.com/doi/pdfdirect/10.1002/chem.202203759Direct link to full text PDF
- Open access
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YesWhether a free full text is available
- OA status
-
hybridOpen access status per OpenAlex
- OA URL
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https://onlinelibrary.wiley.com/doi/pdfdirect/10.1002/chem.202203759Direct OA link when available
- Concepts
-
Norbornadiene, Quadricyclane, Chemistry, X-ray photoelectron spectroscopy, Desorption, Photochemistry, Adsorption, Thermal desorption spectroscopy, Molecule, Thermal desorption, Cyanine, Catalysis, Crystallography, Physical chemistry, Organic chemistry, Physics, Nuclear magnetic resonance, Optics, FluorescenceTop concepts (fields/topics) attached by OpenAlex
- Cited by
-
4Total citation count in OpenAlex
- Citations by year (recent)
-
2024: 2, 2023: 2Per-year citation counts (last 5 years)
- References (count)
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65Number of works referenced by this work
- Related works (count)
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10Other works algorithmically related by OpenAlex
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| abstract_inverted_index.Pt(111) | 72 |
| abstract_inverted_index.X‐ray | 82 |
| abstract_inverted_index.between | 118, 200 |
| abstract_inverted_index.enables | 92 |
| abstract_inverted_index.greater | 54 |
| abstract_inverted_index.induced | 65 |
| abstract_inverted_index.isomers | 166 |
| abstract_inverted_index.overlap | 55 |
| abstract_inverted_index.release | 126 |
| abstract_inverted_index.spectra | 91 |
| abstract_inverted_index.surface | 30, 180 |
| abstract_inverted_index.systems | 212 |
| abstract_inverted_index.thermal | 21 |
| abstract_inverted_index.Abstract | 0 |
| abstract_inverted_index.Ni(111), | 150 |
| abstract_inverted_index.Pt(111). | 136 |
| abstract_inverted_index.allowing | 52 |
| abstract_inverted_index.assessed | 70 |
| abstract_inverted_index.behavior | 205 |
| abstract_inverted_index.catalyst | 77 |
| abstract_inverted_index.compound | 156 |
| abstract_inverted_index.coverage | 181 |
| abstract_inverted_index.derived. | 113 |
| abstract_inverted_index.molecule | 36, 98, 187 |
| abstract_inverted_index.pathways | 162 |
| abstract_inverted_index.sources. | 14 |
| abstract_inverted_index.species. | 197 |
| abstract_inverted_index.suggests | 194 |
| abstract_inverted_index.suitable | 40 |
| abstract_inverted_index.surfaces | 78 |
| abstract_inverted_index.systems. | 23 |
| abstract_inverted_index.achieved, | 51 |
| abstract_inverted_index.catalyzed | 215 |
| abstract_inverted_index.chemistry | 31 |
| abstract_inverted_index.important | 207 |
| abstract_inverted_index.molecular | 19, 147 |
| abstract_inverted_index.necessary | 5 |
| abstract_inverted_index.reactions | 66 |
| abstract_inverted_index.renewable | 12 |
| abstract_inverted_index.solutions | 3 |
| abstract_inverted_index.spectrum. | 59 |
| abstract_inverted_index.thermally | 64 |
| abstract_inverted_index.triggered | 134 |
| abstract_inverted_index.Auspicious | 15 |
| abstract_inverted_index.Comparison | 86 |
| abstract_inverted_index.Monitoring | 114 |
| abstract_inverted_index.Pronounced | 174 |
| abstract_inverted_index.absorption | 48 |
| abstract_inverted_index.adsorption | 62, 109, 201 |
| abstract_inverted_index.candidates | 16 |
| abstract_inverted_index.conversion | 152 |
| abstract_inverted_index.desorption | 175, 204 |
| abstract_inverted_index.framework. | 148 |
| abstract_inverted_index.individual | 160 |
| abstract_inverted_index.processes. | 216 |
| abstract_inverted_index.respective | 89 |
| abstract_inverted_index.transition | 8 |
| abstract_inverted_index.correlation | 199 |
| abstract_inverted_index.counterpart | 102 |
| abstract_inverted_index.derivatized | 34 |
| abstract_inverted_index.distinction | 94 |
| abstract_inverted_index.information | 106 |
| abstract_inverted_index.investigate | 28 |
| abstract_inverted_index.push–pull | 41 |
| abstract_inverted_index.qualitative | 105 |
| abstract_inverted_index.so‐called | 18 |
| abstract_inverted_index.synchrotron | 80 |
| abstract_inverted_index.applications | 209 |
| abstract_inverted_index.bathochromic | 44 |
| abstract_inverted_index.demonstrates | 124 |
| abstract_inverted_index.quantitative | 116 |
| abstract_inverted_index.spectroscopy | 84 |
| abstract_inverted_index.successfully | 133 |
| abstract_inverted_index.Specifically, | 60 |
| abstract_inverted_index.decomposition | 161 |
| abstract_inverted_index.energy‐lean | 101, 186 |
| abstract_inverted_index.energy‐rich | 97, 155 |
| abstract_inverted_index.fragmentation | 144 |
| abstract_inverted_index.photoelectron | 83 |
| abstract_inverted_index.respectively. | 173 |
| abstract_inverted_index.substituents, | 42 |
| abstract_inverted_index.cycloreversion | 117 |
| abstract_inverted_index.heterogeneously | 214 |
| abstract_inverted_index.energy‐storage | 2 |
| abstract_inverted_index.radiation‐based | 81 |
| abstract_inverted_index.spectroscopically | 123 |
| abstract_inverted_index.norbornadiene/quadricyclane | 35 |
| abstract_inverted_index.2‐carbethoxy‐3‐phenyl‐norbornadiene/quadricyclane | 68 |
| cited_by_percentile_year.max | 96 |
| cited_by_percentile_year.min | 94 |
| corresponding_author_ids | https://openalex.org/A5071842639 |
| countries_distinct_count | 1 |
| institutions_distinct_count | 12 |
| corresponding_institution_ids | https://openalex.org/I181369854, https://openalex.org/I75951250 |
| sustainable_development_goals[0].id | https://metadata.un.org/sdg/7 |
| sustainable_development_goals[0].score | 0.8700000047683716 |
| sustainable_development_goals[0].display_name | Affordable and clean energy |
| citation_normalized_percentile.value | 0.5436615 |
| citation_normalized_percentile.is_in_top_1_percent | False |
| citation_normalized_percentile.is_in_top_10_percent | False |