Synthesis and Morphological Control of VO2 Nanostructures via a One-Step Hydrothermal Method Article Swipe
Özlem Karahan
,
Ali Tufani
,
Serkan Ünal
,
I. B. Misirlioglu
,
Yusuf́ Z. Menceloǵlu
,
Kürşat Şendur
·
YOU?
·
· 2021
· Open Access
·
· DOI: https://doi.org/10.3390/nano11030752
YOU?
·
· 2021
· Open Access
·
· DOI: https://doi.org/10.3390/nano11030752
The morphology of nanostructures is a vital parameter to consider in components comprised of materials exhibiting specific functionalities. The number of process steps and the need for high temperatures can often be a limiting factor when targeting a specific morphology. Here, we demonstrate a repeatable synthesis of different morphologies of a highly crystalline monoclinic phase of vanadium dioxide (VO2(M)) using a one-step hydrothermal method. By adjusting the synthesis parameters, such as pH, temperature, and reducing agent concentration in the precursor, VO2 nanostructures with high uniformity and crystallinity are achieved. Some of these morphologies were obtained via the choice of the reducing agent that allowed us to skip the annealing step. Our results indicate that the morphologies of the nanostructures are very sensitive to the hydrazine hydrate (N2H4.H2O) concentration. Another reducing agent, dodecylamine, was used to achieve well-organized and high-quality VO2(M) nanotubes. Differential scanning calorimetry (DSC) experiments revealed that all samples display the monoclinic-to-tetragonal structural transition (MTST) regardless of the morphology, albeit at different temperatures that can be interpreted as the variations in overheating and undercooling limits. VO2(M) structures with a higher surface to volume ratio exhibit a higher overheating limit than those with low ratios.
Related Topics
Concepts
Materials science
Monoclinic crystal system
Differential scanning calorimetry
Crystallinity
Hydrothermal circulation
Hydrothermal synthesis
Chemical engineering
Nanostructure
Reducing agent
Hydrate
Nanotechnology
Tetragonal crystal system
Annealing (glass)
Surface-area-to-volume ratio
Supercooling
Crystal structure
Crystallography
Chemistry
Composite material
Organic chemistry
Thermodynamics
Physics
Engineering
Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.3390/nano11030752
- https://www.mdpi.com/2079-4991/11/3/752/pdf?version=1615953926
- OA Status
- gold
- Cited By
- 33
- References
- 58
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W3138121757
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
-
https://openalex.org/W3138121757Canonical identifier for this work in OpenAlex
- DOI
-
https://doi.org/10.3390/nano11030752Digital Object Identifier
- Title
-
Synthesis and Morphological Control of VO2 Nanostructures via a One-Step Hydrothermal MethodWork title
- Type
-
articleOpenAlex work type
- Language
-
enPrimary language
- Publication year
-
2021Year of publication
- Publication date
-
2021-03-17Full publication date if available
- Authors
-
Özlem Karahan, Ali Tufani, Serkan Ünal, I. B. Misirlioglu, Yusuf́ Z. Menceloǵlu, Kürşat ŞendurList of authors in order
- Landing page
-
https://doi.org/10.3390/nano11030752Publisher landing page
- PDF URL
-
https://www.mdpi.com/2079-4991/11/3/752/pdf?version=1615953926Direct link to full text PDF
- Open access
-
YesWhether a free full text is available
- OA status
-
goldOpen access status per OpenAlex
- OA URL
-
https://www.mdpi.com/2079-4991/11/3/752/pdf?version=1615953926Direct OA link when available
- Concepts
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Materials science, Monoclinic crystal system, Differential scanning calorimetry, Crystallinity, Hydrothermal circulation, Hydrothermal synthesis, Chemical engineering, Nanostructure, Reducing agent, Hydrate, Nanotechnology, Tetragonal crystal system, Annealing (glass), Surface-area-to-volume ratio, Supercooling, Crystal structure, Crystallography, Chemistry, Composite material, Organic chemistry, Thermodynamics, Physics, EngineeringTop concepts (fields/topics) attached by OpenAlex
- Cited by
-
33Total citation count in OpenAlex
- Citations by year (recent)
-
2025: 9, 2024: 7, 2023: 5, 2022: 10, 2021: 2Per-year citation counts (last 5 years)
- References (count)
-
58Number of works referenced by this work
- Related works (count)
-
10Other works algorithmically related by OpenAlex
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