Synthesis, crystal structure, and thermal properties of Ni(NH₃)₄(AFT)₂ Article Swipe

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Shu-Han Wei , Xiao Ma , Zimei Ding , Kang Xu , Hongxu Gao , Jie Huang , Fengqi Zhao ·

YOU? · · 2020 · Open Access · · DOI: https://doi.org/10.1177/1747519820939475

Ni(NH 3 ) 4 (AFT) 2 [NiC 6 H 16 N 18 O 2 , AFT = 4-amino-3-(5-tetrazolate)furazan] is synthesized and characterized by elemental analysis and Fourier-transform infrared spectroscopy for the first time. X-ray diffraction measurements are used to determine the crystal structure of compound 1. The results demonstrate that compound 1 crystallized in the orthorhombic crystal system. The nickel(II) ion is six-coordinated by N atoms from two AFT-ligands and four NH 3 molecules. Its thermal properties are investigated by differential scanning calorimetry and thermogravimetry-derivative thermogravimetry methods, with the results demonstrating that the differential scanning calorimetry curve exhibits two endothermic and one exothermic processes. The endothermic processes are in the range of 130–510 °C with a peak temperature of 188 °C. The temperature from 230 to 400 °C is the exothermic process in which the peak temperature is 314.58 °C. In addition, Kissinger’s and Ozawa-Doyle’s methods are used for calculating the non-isothermal kinetics parameters. Moreover, the apparent activation energy ( E), safety, and thermal stability parameters ( T SADT , T TIT , T b ) for Ni(NH 3 ) 4 (AFT) 2 are calculated. In addition, the calculated thermodynamic functions ( ∆S ≠ , ∆H ≠ , and ∆G ≠ ) for the exothermic decomposition process of Ni(NH 3 ) 4 (AFT) 2 are 55.07 J mol −1 K −1 , 196.18 kJ mol −1 , and 164.90 kJ mol −1 , respectively.

Related Topics

Thermogravimetric Analysis

Differential Scanning Calorimetry

Exothermic Reaction

Exothermic Process

Crystal Structure

Diurnal Air Temperature Variation

Crystallography

Chemistry

Infrared Spectroscopy

Crystal (Programming Language)

$Diffraction$

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Thermogravimetry Endothermic process Orthorhombic crystal system Differential scanning calorimetry Exothermic reaction Exothermic process Thermal decomposition Crystal structure Atmospheric temperature range Thermal stability Differential thermal analysis Crystallography Thermal analysis Isothermal process Chemistry Analytical Chemistry (journal) Infrared spectroscopy Crystal (programming language) Activation energy Physical chemistry Inorganic chemistry Thermodynamics Thermal Adsorption Diffraction Organic chemistry Computer science Optics Physics Programming language

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Landing Page: https://doi.org/10.1177/1747519820939475
PDF: https://journals.sagepub.com/doi/pdf/10.1177/1747519820939475
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Title: Synthesis, crystal structure, and thermal properties of Ni(NH₃)₄(AFT)₂

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Publication year: 2020

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Publication date: 2020-07-26

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Authors: Shu-Han Wei, Xiao Ma, Zimei Ding, Kang Xu, Hongxu Gao, Jie Huang, Fengqi Zhao

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Landing page: https://doi.org/10.1177/1747519820939475

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Concepts: Thermogravimetry, Endothermic process, Orthorhombic crystal system, Differential scanning calorimetry, Exothermic reaction, Exothermic process, Thermal decomposition, Crystal structure, Atmospheric temperature range, Thermal stability, Differential thermal analysis, Crystallography, Thermal analysis, Isothermal process, Chemistry, Analytical Chemistry (journal), Infrared spectroscopy, Crystal (programming language), Activation energy, Physical chemistry, Inorganic chemistry, Thermodynamics, Thermal, Adsorption, Diffraction, Organic chemistry, Computer science, Optics, Physics, Programming language

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Synthesis, crystal structure, and thermal properties of Ni(NH₃)₄(AFT)₂ Article Swipe