Synthesis of Mo4VAlC4 MAX Phase and Two-Dimensional Mo4VC4 MXene with Five Atomic Layers of Transition Metals Article Swipe

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Grayson Deysher , Christopher E. Shuck , Kanit Hantanasirisakul , Nathan C. Frey , Alexandre C. Foucher , Kathleen Maleski , Asia Sarycheva , Vivek B. Shenoy , Eric A. Stach , Babak Anasori , Yury Gogotsi ·

YOU? · · 2023 · Open Access · · DOI: https://doi.org/10.1201/9781003306511-8

MXenes are a family of two-dimensional (2D) transition\nmetal carbides,\nnitrides, and carbonitrides with a general formula of M_n+1X_nT_x, in which two, three, or four atomic layers of a transition\nmetal (M: Ti, Nb, V, Cr, Mo, Ta, etc.) are interleaved with layers\nof C and/or N (shown as X), and T_x represents\nsurface termination groups such as −OH, O, and −F.\nHere, we report the scalable synthesis and characterization of a MXene\nwith five atomic layers of transition metals (Mo₄VC₄T_x), by synthesizing its Mo₄VAlC₄ MAX phase precursor that contains no other\nMAX phase impurities. These phases display twinning at their central\nM layers which is not present in any other known MAX phases or MXenes.\nTransmission electron microscopy and X-ray diffraction were used to\nexamine the structure of both phases. Energy-dispersive X-ray spectroscopy,\nX-ray photoelectron spectroscopy, Raman spectroscopy, and high-resolution\nscanning transmission electron microscopy with energy-dispersive X-ray\nspectroscopy were used to study the composition of these materials.\nDensity functional theory calculations indicate that other five transition\nmetal-layer MAX phases (M′₄M″AlC₄) may be possible, where M′ and M″ are two different\ntransition metals. The predicted existence of additional Al-containing\nMAX phases suggests that more M₅C₄T_x MXenes can be synthesized. Additionally, we characterized\nthe optical, electronic, and thermal properties of Mo₄VC₄T_x. This study demonstrates the\nexistence of an additional subfamily of M₅X₄T_x MXenes as well as a twinned structure,\nallowing for a wider range of 2D structures and compositions for more\ncontrol over properties, which could lead to many different applications.

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Transition metal Materials science Chemistry Chemical physics Catalysis Organic chemistry

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Type: book-chapter
Language: en
Landing Page: https://doi.org/10.1201/9781003306511-8
OA Status: green
Cited By: 12
Related Works: 10
OpenAlex ID: https://openalex.org/W4380052860

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OpenAlex ID: https://openalex.org/W4380052860

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DOI: https://doi.org/10.1201/9781003306511-8

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Title: Synthesis of Mo4VAlC4 MAX Phase and Two-Dimensional Mo4VC4 MXene with Five Atomic Layers of Transition Metals

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Type: book-chapter

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Language: en

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Publication year: 2023

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Publication date: 2023-06-08

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Authors: Grayson Deysher, Christopher E. Shuck, Kanit Hantanasirisakul, Nathan C. Frey, Alexandre C. Foucher, Kathleen Maleski, Asia Sarycheva, Vivek B. Shenoy, Eric A. Stach, Babak Anasori, Yury Gogotsi

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Landing page: https://doi.org/10.1201/9781003306511-8

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OA URL: https://figshare.com/articles/journal_contribution/Synthesis_of_Mo_sub_4_sub_VAlC_sub_4_sub_MAX_Phase_and_Two-Dimensional_Mo_sub_4_sub_VC_sub_4_sub_MXene_with_Five_Atomic_Layers_of_Transition_Metals/11385498

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Concepts: Transition metal, Materials science, Chemistry, Chemical physics, Catalysis, Organic chemistry

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Cited by: 12

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Citations by year (recent): 2025: 2, 2024: 2, 2023: 2, 2022: 3, 2021: 2

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Related works (count): 10

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abstract_inverted_index.Mo<sub>4</sub>VAlC<sub>4</sub>	77
abstract_inverted_index.(M′<sub>4</sub>M″AlC<sub>4</sub>)	154
abstract_inverted_index.M<sub>5</sub>C<sub>4</sub>T<sub><i>x</i></sub>	176
abstract_inverted_index.M<sub>5</sub>X<sub>4</sub>T<sub><i>x</i></sub>	200
abstract_inverted_index.Mo<sub>4</sub>VC<sub>4</sub>T<sub><i>x</i></sub>.	190
abstract_inverted_index.(Mo<sub>4</sub>VC<sub>4</sub>T<sub><i>x</i></sub>),	73
abstract_inverted_index.M<sub><i>n</i>+1</sub>X<sub><i>n</i></sub>T<sub><i>x</i></sub>,	16
cited_by_percentile_year.max	97
cited_by_percentile_year.min	89
countries_distinct_count	0
institutions_distinct_count	11
citation_normalized_percentile.value	0.9562208
citation_normalized_percentile.is_in_top_1_percent	False
citation_normalized_percentile.is_in_top_10_percent	True