Synthesizing Amorphous Precursors Through Control of Local Composition Article Swipe
Hannah R. Blackwood
,
Annalise Walker
,
David C. Johnson
·
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.26434/chemrxiv-2023-3818h
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.26434/chemrxiv-2023-3818h
Synthesizing compounds predicted to have exceptional properties that are close to or below the ground state convex hull has proven to be very challenging, as avoiding the formation of more thermodynamically or kinetically stable mixtures of known compounds is often required. A homogenous amorphous phase has been suggested as a very general reaction intermediate. However, the preparation of amorphous phases of controlled composition is also very challenging. We postulated that amorphous intermediates with controlled composition can be made by avoiding the formation of regions with compositions close to that of the known compounds. Specifically, we demonstrated that we could avoid the formation of PbSe and MoSe2 by sequentially depositing nonstoichiometric ultrathin sub-monolayer thickness layers on a nominally room temperature substrate. The substrate temperature needs to be low enough to minimize surface diffusion, preventing agglomeration of elements and resultant concentration gradients. The amount of diffusion required to form nucleation embryos can be controlled by changing the difference between the composition of the film and the stoichiometry of the compound in question. Large enough differences should result in amorphous intermediates in most systems. The presence of more than two elements will further suppress the nucleation of binary compounds, making this approach particularly useful to prepare amorphous precursors for the synthesis of metastable ternary and quaternary compounds.
Related Topics
Concepts
Amorphous solid
Nucleation
Ternary operation
Metastability
Substrate (aquarium)
Stoichiometry
Materials science
Diffusion
Chemical physics
Chemical engineering
Composition (language)
Economies of agglomeration
Monolayer
Chemistry
Crystallography
Nanotechnology
Organic chemistry
Thermodynamics
Geology
Programming language
Philosophy
Linguistics
Oceanography
Engineering
Computer science
Physics
Metadata
- Type
- preprint
- Language
- en
- Landing Page
- https://doi.org/10.26434/chemrxiv-2023-3818h
- https://chemrxiv.org/engage/api-gateway/chemrxiv/assets/orp/resource/item/6542db4548dad23120e3ea65/original/synthesizing-amorphous-precursors-through-control-of-local-composition.pdf
- OA Status
- gold
- Cited By
- 1
- References
- 40
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4388298585
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
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https://openalex.org/W4388298585Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.26434/chemrxiv-2023-3818hDigital Object Identifier
- Title
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Synthesizing Amorphous Precursors Through Control of Local CompositionWork title
- Type
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preprintOpenAlex work type
- Language
-
enPrimary language
- Publication year
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2023Year of publication
- Publication date
-
2023-11-03Full publication date if available
- Authors
-
Hannah R. Blackwood, Annalise Walker, David C. JohnsonList of authors in order
- Landing page
-
https://doi.org/10.26434/chemrxiv-2023-3818hPublisher landing page
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https://chemrxiv.org/engage/api-gateway/chemrxiv/assets/orp/resource/item/6542db4548dad23120e3ea65/original/synthesizing-amorphous-precursors-through-control-of-local-composition.pdfDirect link to full text PDF
- Open access
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YesWhether a free full text is available
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goldOpen access status per OpenAlex
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https://chemrxiv.org/engage/api-gateway/chemrxiv/assets/orp/resource/item/6542db4548dad23120e3ea65/original/synthesizing-amorphous-precursors-through-control-of-local-composition.pdfDirect OA link when available
- Concepts
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Amorphous solid, Nucleation, Ternary operation, Metastability, Substrate (aquarium), Stoichiometry, Materials science, Diffusion, Chemical physics, Chemical engineering, Composition (language), Economies of agglomeration, Monolayer, Chemistry, Crystallography, Nanotechnology, Organic chemistry, Thermodynamics, Geology, Programming language, Philosophy, Linguistics, Oceanography, Engineering, Computer science, PhysicsTop concepts (fields/topics) attached by OpenAlex
- Cited by
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1Total citation count in OpenAlex
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2023: 1Per-year citation counts (last 5 years)
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40Number of works referenced by this work
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10Other works algorithmically related by OpenAlex
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| referenced_works | https://openalex.org/W2174924140, https://openalex.org/W2037515859, https://openalex.org/W1969683161, https://openalex.org/W2801403847, https://openalex.org/W1982210646, https://openalex.org/W2025421556, https://openalex.org/W2062434337, https://openalex.org/W2081016721, https://openalex.org/W4243630763, https://openalex.org/W2045861769, https://openalex.org/W2009178744, https://openalex.org/W2035824223, https://openalex.org/W2002162440, https://openalex.org/W2088140356, https://openalex.org/W4293758702, https://openalex.org/W1983283966, https://openalex.org/W1978005636, https://openalex.org/W2009691322, https://openalex.org/W2047193614, https://openalex.org/W2095571376, https://openalex.org/W1984312308, https://openalex.org/W2056473244, https://openalex.org/W2056782397, https://openalex.org/W4320516869, https://openalex.org/W1964212721, https://openalex.org/W808269236, https://openalex.org/W2033802591, https://openalex.org/W2462235801, https://openalex.org/W3081344625, https://openalex.org/W2910949563, https://openalex.org/W2086713312, https://openalex.org/W2886262125, https://openalex.org/W3048481686, https://openalex.org/W2950421303, https://openalex.org/W2030351452, https://openalex.org/W1940906599, https://openalex.org/W4388298585, https://openalex.org/W2042801740, https://openalex.org/W1963891133, https://openalex.org/W3179762655 |
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