The effect of inversion of the ester group on the mesophase behaviour of some azo/ester compounds Article Swipe
Magdi M. Naoum
,
Abdelgawad A. Fahmi
,
Nagwa H.S. Ahmed
,
Gamal R. Saad
·
YOU?
·
· 2015
· Open Access
·
· DOI: https://doi.org/10.1080/02678292.2015.1048754
YOU?
·
· 2015
· Open Access
·
· DOI: https://doi.org/10.1080/02678292.2015.1048754
Five homologous series of 4-substituted phenyl 4′-(4″-alkoxy phenylazo) benzoates (Ina–−e) were prepared in which, within each homologous series, the length of the terminal alkoxy group varies between 8, 10, 12, 14 and 16 carbons, while the other terminal substituent, X, is a polar group that alternatively changed from CH3O, CH3, H, Br, and CN groups. Compounds prepared were characterised by infrared, mass, and H1-NMR spectroscopy and their mesophase behaviour investigated by differential scanning calorimetry (DSC) and polarised light microscopy (PLM). The results were discussed in terms of mesomeric and polarisability effects. Only for the lower group of compounds, I8a-e, that showed a nematic phase, the nematic-to-isotropic transition temperatures (TN–I) were successfully correlated to the polarisability anisotropy of bonds to the substituent X. A comparative study was made between the investigated compounds and two previously prepared isomeric groups. In the first group of isomers, 4-(4′alkoxy phenylazo) phenyl 4″-substituted benzoates (IIna–e), the ester groups are inverted. While in the second, 4-(4′-substituted phenylazo) phenyl 4″-alkoxy benzoates (IIIna–e), two modifications were made, inversion of the COO group, and exchange of the two wing substituents
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- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1080/02678292.2015.1048754
- OA Status
- green
- Cited By
- 40
- References
- 34
- Related Works
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- OpenAlex ID
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All OpenAlex metadata
Raw OpenAlex JSON
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https://openalex.org/W2137568580Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.1080/02678292.2015.1048754Digital Object Identifier
- Title
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The effect of inversion of the ester group on the mesophase behaviour of some azo/ester compoundsWork title
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articleOpenAlex work type
- Language
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enPrimary language
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2015Year of publication
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2015-07-02Full publication date if available
- Authors
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Magdi M. Naoum, Abdelgawad A. Fahmi, Nagwa H.S. Ahmed, Gamal R. SaadList of authors in order
- Landing page
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https://doi.org/10.1080/02678292.2015.1048754Publisher landing page
- Open access
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YesWhether a free full text is available
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greenOpen access status per OpenAlex
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https://figshare.com/articles/journal_contribution/The_effect_of_inversion_of_the_ester_group_on_the_mesophase_behaviour_of_some_azo_ester_compounds/1471605Direct OA link when available
- Concepts
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Benzoates, Homologous series, Alkoxy group, Mesophase, Substituent, Liquid crystal, Differential scanning calorimetry, Crystallography, Infrared spectroscopy, Alkyl, Stereochemistry, Materials science, Medicinal chemistry, Chemistry, Organic chemistry, Thermodynamics, Physics, OptoelectronicsTop concepts (fields/topics) attached by OpenAlex
- Cited by
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40Total citation count in OpenAlex
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2025: 3, 2023: 3, 2022: 3, 2021: 6, 2020: 6Per-year citation counts (last 5 years)
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34Number of works referenced by this work
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10Other works algorithmically related by OpenAlex
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