Thermal analysis: basic concept of differential scanning calorimetry and thermogravimetry for beginners Article Swipe
N. F. A. Zainal
,
Jean Marc Saiter
,
Suhaila Idayu Abdul Halim
,
Romain Lucas
,
Chin Han Chan
·
YOU?
·
· 2020
· Open Access
·
· DOI: https://doi.org/10.1515/cti-2020-0010
YOU?
·
· 2020
· Open Access
·
· DOI: https://doi.org/10.1515/cti-2020-0010
We present an overview for the basic fundamental of thermal analysis, which is applicable for educational purposes, especially for lecturers at the universities, who may refer to the articles as the references to “teach” or to “lecture” to final year project students or young researchers who are working on their postgraduate projects. Description of basic instrumentation [ i.e. differential scanning calorimetry (DSC) and thermogravimetry (TGA)] covers from what we should know about the instrument, calibration, baseline and samples’ signal. We also provide the step-by-step guides for the estimation of the glass transition temperature after DSC as well as examples and exercises are included, which are applicable for teaching activities. Glass transition temperature is an important property for commercial application of a polymeric material, e.g. packaging, automotive, etc. TGA is also highlighted where the analysis gives important thermal degradation information of a material to avoid sample decomposition during the DSC measurement. The step-by-step guides of the estimation of the activation energy after TGA based on Hoffman’s Arrhenius-like relationship are also provided.
Related Topics
Concepts
Thermogravimetry
Differential scanning calorimetry
Glass transition
Instrumentation (computer programming)
Thermal analysis
Process engineering
Calorimetry
Sample (material)
Thermal decomposition
Materials science
Computer science
Thermal
Analytical Chemistry (journal)
Chemistry
Thermodynamics
Physics
Chemical engineering
Composite material
Engineering
Polymer
Organic chemistry
Programming language
Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1515/cti-2020-0010
- https://www.degruyter.com/document/doi/10.1515/cti-2020-0010/pdf
- OA Status
- gold
- Cited By
- 29
- References
- 16
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W3109745042
All OpenAlex metadata
Raw OpenAlex JSON
- OpenAlex ID
-
https://openalex.org/W3109745042Canonical identifier for this work in OpenAlex
- DOI
-
https://doi.org/10.1515/cti-2020-0010Digital Object Identifier
- Title
-
Thermal analysis: basic concept of differential scanning calorimetry and thermogravimetry for beginnersWork title
- Type
-
articleOpenAlex work type
- Language
-
enPrimary language
- Publication year
-
2020Year of publication
- Publication date
-
2020-11-26Full publication date if available
- Authors
-
N. F. A. Zainal, Jean Marc Saiter, Suhaila Idayu Abdul Halim, Romain Lucas, Chin Han ChanList of authors in order
- Landing page
-
https://doi.org/10.1515/cti-2020-0010Publisher landing page
- PDF URL
-
https://www.degruyter.com/document/doi/10.1515/cti-2020-0010/pdfDirect link to full text PDF
- Open access
-
YesWhether a free full text is available
- OA status
-
goldOpen access status per OpenAlex
- OA URL
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https://www.degruyter.com/document/doi/10.1515/cti-2020-0010/pdfDirect OA link when available
- Concepts
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Thermogravimetry, Differential scanning calorimetry, Glass transition, Instrumentation (computer programming), Thermal analysis, Process engineering, Calorimetry, Sample (material), Thermal decomposition, Materials science, Computer science, Thermal, Analytical Chemistry (journal), Chemistry, Thermodynamics, Physics, Chemical engineering, Composite material, Engineering, Polymer, Organic chemistry, Programming languageTop concepts (fields/topics) attached by OpenAlex
- Cited by
-
29Total citation count in OpenAlex
- Citations by year (recent)
-
2025: 8, 2024: 11, 2023: 5, 2022: 5Per-year citation counts (last 5 years)
- References (count)
-
16Number of works referenced by this work
- Related works (count)
-
10Other works algorithmically related by OpenAlex
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