Two Birds with One Stone: Ammonium-Induced Carbon Nanotube Structure and Low-Crystalline Cobalt Nanoparticles Enabling High Performance of Lithium-Sulfur Batteries Article Swipe
Qi Tan
,
Hongliang Liu
,
Guozhu Liang
,
Kaigui Jiang
,
Hangxuan Xie
,
Weijie Si
,
Jiajv Lin
,
Xiongwu Kang
·
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.3390/inorganics11070305
YOU?
·
· 2023
· Open Access
·
· DOI: https://doi.org/10.3390/inorganics11070305
The electrochemical performance of lithium–sulfur batteries (LiSBs) has been hampered by the slow redox kinetics and shuttle effect of lithium polysulfides (LiPSs), which require the rational design and synthesis of highly active electrocatalysts towards this reaction. Herein, worm-like N-doped porous carbon nanotube-supported low-crystalline Co nanoparticles (a-Co-NC@C) were derived from binary Zn–Co ZIF via a two-step thermal annealing method. Initial thermal annealing 950 °C in Ar + H2 atmosphere results in the carbonization of binary Zn–Co ZIF and the formation of high crystalline Co nanoparticles. Thermal annealing in ammonia atmosphere at 350 °C not only results in the reduced crystallinity of cobalt nanoparticles; it also promotes the growth of highly graphitized and heavily N-doped intertwined carbon nanotubes. The enlarged porous carbon nanotube structure offers accommodation for sulfur content, while the doped carbon and Co nanoparticles with reduced crystallinity facilitate the redox kinetics of LiPSs, improving the cycling stability, rate performance and capacity of LiSBs batteries. As a result, the a-Co-NC@C cathode displays a specific capacity of 559 mAh g−1 after 500 cycles at 1 C, and a specific capacity of 572 mAh g−1 at 3 C. It delivers a specific capacity of 579 mAh g−1 at high sulfur loading of a 2.55 mg cm−2 at 1 C after 400 cycles. This work highlights the importance of phase engineering of carbon matrix and transition metal nanoparticles in electrochemical performance of Li-S batteries.
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- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.3390/inorganics11070305
- https://www.mdpi.com/2304-6740/11/7/305/pdf?version=1689727271
- OA Status
- gold
- Cited By
- 4
- References
- 39
- Related Works
- 10
- OpenAlex ID
- https://openalex.org/W4384828072
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Raw OpenAlex JSON
- OpenAlex ID
-
https://openalex.org/W4384828072Canonical identifier for this work in OpenAlex
- DOI
-
https://doi.org/10.3390/inorganics11070305Digital Object Identifier
- Title
-
Two Birds with One Stone: Ammonium-Induced Carbon Nanotube Structure and Low-Crystalline Cobalt Nanoparticles Enabling High Performance of Lithium-Sulfur BatteriesWork title
- Type
-
articleOpenAlex work type
- Language
-
enPrimary language
- Publication year
-
2023Year of publication
- Publication date
-
2023-07-18Full publication date if available
- Authors
-
Qi Tan, Hongliang Liu, Guozhu Liang, Kaigui Jiang, Hangxuan Xie, Weijie Si, Jiajv Lin, Xiongwu KangList of authors in order
- Landing page
-
https://doi.org/10.3390/inorganics11070305Publisher landing page
- PDF URL
-
https://www.mdpi.com/2304-6740/11/7/305/pdf?version=1689727271Direct link to full text PDF
- Open access
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YesWhether a free full text is available
- OA status
-
goldOpen access status per OpenAlex
- OA URL
-
https://www.mdpi.com/2304-6740/11/7/305/pdf?version=1689727271Direct OA link when available
- Concepts
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Materials science, Crystallinity, Chemical engineering, Carbon nanotube, Nanoparticle, Cobalt, Electrochemistry, Thermal treatment, Annealing (glass), Nanotechnology, Inorganic chemistry, Electrode, Chemistry, Composite material, Physical chemistry, Engineering, MetallurgyTop concepts (fields/topics) attached by OpenAlex
- Cited by
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4Total citation count in OpenAlex
- Citations by year (recent)
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2025: 1, 2024: 2, 2023: 1Per-year citation counts (last 5 years)
- References (count)
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39Number of works referenced by this work
- Related works (count)
-
10Other works algorithmically related by OpenAlex
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