Understanding the Effect of Lithium Nitrate as Additive in Carbonate-Based Electrolytes for Silicon Anodes Article Swipe
Maximilian Graf
,
Lennart Reuter
,
Simon Qian
,
Tom Calmus
,
Rebecca Bernhard
,
Stefan Haufe
,
Hubert A. Gasteiger
·
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.1149/1945-7111/ad71f7
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.1149/1945-7111/ad71f7
Due to its high specific capacity, silicon is one of the most promising anode materials for next-generation lithium-ion batteries. However, its large volumetric changes upon (de)lithiation of ∼300% lead to a rupture/re-formation of the solid-electrolyte interphase (SEI) upon cycling, resulting in continuous electrolyte consumption and irreversible loss of lithium. Therefore, it is crucial to use electrolyte systems that form a more stable SEI that can withstand large volume changes. Here, we investigate lithium nitrate (LiNO 3 ) and lithium nitrite (LiNO 2 ) as electrolyte additives. Linear scan voltammetry on carbon black working electrodes in a half-cell configuration with LiNO 3 -containing 1 M LiPF 6 in EC/DEC (1/2 v/v) revealed a two-step reduction mechanism, whereby the first reduction peak could be attributed to the conversion of LiNO 3 to LiNO 2 , while X-ray photoelectron spectroscopy on harvested electrodes suggests the formation of Li 3 N during the second reduction peak. On-line electrochemical mass spectrometry (OEMS) on carbon black electrodes showed that N 2 O gas is evolved upon the reduction of LiNO 3 - and LiNO 2 -containing electrolytes but that the gassing associated with EC reduction is significantly reduced. Furthermore, OEMS and voltammetry were used to examine the redox chemistry of LiNO 2 additive. Finally, LiNO 3 and LiNO 2 additives significantly improved the cycle-life of Si||NCM622 full-cells.
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Metadata
- Type
- article
- Language
- en
- Landing Page
- https://doi.org/10.1149/1945-7111/ad71f7
- OA Status
- hybrid
- Cited By
- 7
- References
- 53
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- 10
- OpenAlex ID
- https://openalex.org/W4402626932
All OpenAlex metadata
Raw OpenAlex JSON
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https://openalex.org/W4402626932Canonical identifier for this work in OpenAlex
- DOI
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https://doi.org/10.1149/1945-7111/ad71f7Digital Object Identifier
- Title
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Understanding the Effect of Lithium Nitrate as Additive in Carbonate-Based Electrolytes for Silicon AnodesWork title
- Type
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articleOpenAlex work type
- Language
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enPrimary language
- Publication year
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2024Year of publication
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2024-09-02Full publication date if available
- Authors
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Maximilian Graf, Lennart Reuter, Simon Qian, Tom Calmus, Rebecca Bernhard, Stefan Haufe, Hubert A. GasteigerList of authors in order
- Landing page
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https://doi.org/10.1149/1945-7111/ad71f7Publisher landing page
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YesWhether a free full text is available
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-
hybridOpen access status per OpenAlex
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https://doi.org/10.1149/1945-7111/ad71f7Direct OA link when available
- Concepts
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Electrolyte, Anode, Lithium nitrate, Lithium (medication), Lithium carbonate, Silicon, Carbonate, Nitrate, Inorganic chemistry, Materials science, Chemical engineering, Chemistry, Ion, Metallurgy, Electrode, Ionic bonding, Organic chemistry, Physical chemistry, Medicine, Endocrinology, EngineeringTop concepts (fields/topics) attached by OpenAlex
- Cited by
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7Total citation count in OpenAlex
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2025: 6, 2024: 1Per-year citation counts (last 5 years)
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10Other works algorithmically related by OpenAlex
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| referenced_works | https://openalex.org/W2028872506, https://openalex.org/W2622680715, https://openalex.org/W2758193105, https://openalex.org/W2067584365, https://openalex.org/W1982702179, https://openalex.org/W2419336826, https://openalex.org/W2537935631, https://openalex.org/W4320890756, https://openalex.org/W2955355207, https://openalex.org/W2745596162, https://openalex.org/W2883384770, https://openalex.org/W2332009222, https://openalex.org/W2254621427, https://openalex.org/W2413726566, https://openalex.org/W3135882425, https://openalex.org/W3025473585, https://openalex.org/W3194985186, https://openalex.org/W2777639606, https://openalex.org/W2057899803, https://openalex.org/W2324219433, https://openalex.org/W3103145957, https://openalex.org/W2887725221, https://openalex.org/W2957925434, https://openalex.org/W2092146792, https://openalex.org/W1782726582, https://openalex.org/W4248899822, https://openalex.org/W2991536910, https://openalex.org/W2278913458, https://openalex.org/W2069154361, https://openalex.org/W2313604584, https://openalex.org/W3181366049, https://openalex.org/W2565607787, https://openalex.org/W2943671090, https://openalex.org/W2934875772, https://openalex.org/W2314119111, https://openalex.org/W2749900974, https://openalex.org/W2052909548, https://openalex.org/W4399831498, https://openalex.org/W1952370507, https://openalex.org/W2341583297, https://openalex.org/W2949094692, https://openalex.org/W2059481908, https://openalex.org/W2735041121, https://openalex.org/W1985836543, https://openalex.org/W4366442075, https://openalex.org/W2753293769, https://openalex.org/W2797321974, https://openalex.org/W2611622996, https://openalex.org/W3098103185, https://openalex.org/W171773285, https://openalex.org/W2046611473, https://openalex.org/W2803789241, https://openalex.org/W2087758007 |
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