Unraveling nano-scale effects of topotactic reduction in LaNiO2 crystals Article Swipe
Yu‐Mi Wu
,
Pascal Puphal
,
Masahiko Isobe
,
B. Keimer
,
Matthias Hepting
,
Y. Eren Suyolcu
,
Peter A. van Aken
·
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.1063/5.0227732
YOU?
·
· 2024
· Open Access
·
· DOI: https://doi.org/10.1063/5.0227732
Infinite-layer nickelates stand as a promising frontier in the exploration of unconventional superconductivity. Their synthesis through topotactic oxygen reduction from the parent perovskite phase remains a complex and elusive process. This study delves into the nano-scale effects of the topotactic lattice transformation within LaNiO2 crystals. Leveraging high-resolution scanning transmission electron microscopy and spectroscopy, our investigations uncover a panorama of structural alterations, including grain boundaries and coherent twin boundaries, triggered by reduction-induced transformations. In addition, our analyses unveil the formation of an oxygen-rich disordered transition phase encircling impurities and pervading crystalline domains and the internal strain is accommodated by grain boundary formation. By unraveling these nano-scale effects, our findings provide insights into the microscopic intricacies of the topotactic reduction process elucidating the transition from the perovskite to the infinite-layer phase within nickelate bulk crystals.
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All OpenAlex metadata
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Unraveling nano-scale effects of topotactic reduction in LaNiO2 crystalsWork title
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enPrimary language
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2024Year of publication
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2024-09-01Full publication date if available
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Yu‐Mi Wu, Pascal Puphal, Masahiko Isobe, B. Keimer, Matthias Hepting, Y. Eren Suyolcu, Peter A. van AkenList of authors in order
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https://doi.org/10.1063/5.0227732Publisher landing page
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goldOpen access status per OpenAlex
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1Total citation count in OpenAlex
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