Andrew M. Minor
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View article: Modification of Ni-20Cr corrosion dealloying behavior in molten fluorides via cold work induced plastic deformation
Modification of Ni-20Cr corrosion dealloying behavior in molten fluorides via cold work induced plastic deformation Open
The corrosion dealloying behavior of cold-worked (CW) Ni20Cr alloy (wt%) was studied in molten LiF-NaF-KF (or FLiNaK) salts at 600 °C, equal to a homologous temperature (T H) of 0.52. Alloys were cold-rolled to achieve reductions of thickn…
View article: New avenues for characterizing individual mineralized collagen fibrils with transmission electron microscopy
New avenues for characterizing individual mineralized collagen fibrils with transmission electron microscopy Open
Bone serves as a remarkable example of nature's architectured material with its unique blend of strength and toughness, all at a lightweight design. Given the hierarchical nature of these materials, it is essential to understand the govern…
View article: In Situ 4D‐STEM Imaging of the Orientation of Lamellar Clusters in Polymer Crystallization
In Situ 4D‐STEM Imaging of the Orientation of Lamellar Clusters in Polymer Crystallization Open
View article: Tiny Bubbles: Combined HR(S)TEM and 4D-STEM Analysis of Sub-Nanometer He Bubbles in Au
Tiny Bubbles: Combined HR(S)TEM and 4D-STEM Analysis of Sub-Nanometer He Bubbles in Au Open
Irradiation produces a distribution of defect sizes in materials, with the smallest defects often below one nanometer in size and approaching the scale of a single unit cell in metals. While high-resolution scanning transmission electron m…
View article: Uncovering the re-distribution mechanism of Ni in a de-alloyed Ni-Cr alloy in molten fluorinated salts
Uncovering the re-distribution mechanism of Ni in a de-alloyed Ni-Cr alloy in molten fluorinated salts Open
A mechanism of Ni redeposition during dealloying corrosion of Ni-Cr is investigated. A model Ni20Cr (wt%) metal alloy was exposed to molten LiF-NaF-KF eutectic (FLiNaK) at 600 °C and at an applied potential of +2.1 V K+/K , above the criti…
View article: Correction: Materials laboratories of the future for alloys, amorphous, and composite materials
Correction: Materials laboratories of the future for alloys, amorphous, and composite materials Open
View article: π–π Stacking in Kerogen and Its Mechanical Impact
π–π Stacking in Kerogen and Its Mechanical Impact Open
Kerogen is a key source of hydrocarbon production through hydraulic fracturing. However, the direct correlation between the molecular structure and mechanical properties remains unclear. Here, we employ four-dimensional scanning transmissi…
View article: Materials laboratories of the future for alloys, amorphous, and composite materials
Materials laboratories of the future for alloys, amorphous, and composite materials Open
In alignment with the Materials Genome Initiative and as the product of a workshop sponsored by the US National Science Foundation, we define a vision for materials laboratories of the future in alloys, amorphous materials, and composite m…
View article: Dynamics and structure of the B2→B19’ phase transformation in NiTi revealed through in situ 4D-STEM
Dynamics and structure of the B2→B19’ phase transformation in NiTi revealed through in situ 4D-STEM Open
View article: Self-Heating Conductive Ceramic Composites for High Temperature Thermal Energy Storage
Self-Heating Conductive Ceramic Composites for High Temperature Thermal Energy Storage Open
The absence of affordable and deployable large-scale energy storage poses a major barrier to providing zero-emission energy on demand for societal decarbonization. High temperature thermal energy storage is one promising option with low co…
View article: Si/Ge<mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML" altimg="si16.svg" display="inline" id="d1e239"><mml:msub><mml:mrow/><mml:mrow><mml:mn>1</mml:mn><mml:mo>−</mml:mo><mml:mi>x</mml:mi></mml:mrow></mml:msub></mml:math>Sn<mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML" altimg="si17.svg" display="inline" id="d1e251"><mml:msub><mml:mrow/><mml:mrow><mml:mi>x</mml:mi></mml:mrow></mml:msub></mml:math>/Si transistors with highly transparent Al contacts
Si/GeSn/Si transistors with highly transparent Al contacts Open
View article: Temperature-dependent electronic transport in reconfigurable transistors based on Ge on SOI and strained SOI platforms
Temperature-dependent electronic transport in reconfigurable transistors based on Ge on SOI and strained SOI platforms Open
View article: Ballistic ion transport through hierarchically-ordered-structure polymer binder
Ballistic ion transport through hierarchically-ordered-structure polymer binder Open
Achieving ballistic ion transport in a mixed electronic-ionic conductive polymer, its hierarchically ordered structure (HOS) facilitates ion diffusion and results in solid-state Li + conductivity in the range of 10 −4 to 10 −3 S cm −1 from…
View article: Dealloying of Cold-Worked Ni-20Cr (wt.%) Alloys In&nbsp;Molten LiF-NaF-KF Salts
Dealloying of Cold-Worked Ni-20Cr (wt.%) Alloys In Molten LiF-NaF-KF Salts Open
View article: High-temperature carbon dioxide capture in a porous material with terminal zinc hydride sites
High-temperature carbon dioxide capture in a porous material with terminal zinc hydride sites Open
Carbon capture can mitigate point-source carbon dioxide (CO 2 ) emissions, but hurdles remain that impede the widespread adoption of amine-based technologies. Capturing CO 2 at temperatures closer to those of many industrial exhaust stream…
View article: Unraveling Interdiffusion Phenomena and the Role of Nanoscale Diffusion Barriers in the Copper–Gold System
Unraveling Interdiffusion Phenomena and the Role of Nanoscale Diffusion Barriers in the Copper–Gold System Open
Diffusion is one of the most fundamental concepts in materials science, playing a pivotal role in materials synthesis, forming, and degradation. Of particular importance is solid state interdiffusion of metals which defines the usable para…
View article: The hierarchical structure of organic mixed ionic–electronic conductors and its evolution in water
The hierarchical structure of organic mixed ionic–electronic conductors and its evolution in water Open
View article: The 4D Camera: An 87 kHz Direct Electron Detector for Scanning/Transmission Electron Microscopy
The 4D Camera: An 87 kHz Direct Electron Detector for Scanning/Transmission Electron Microscopy Open
We describe the development, operation, and application of the 4D Camera—a 576 by 576 pixel active pixel sensor for scanning/transmission electron microscopy which operates at 87,000 Hz. The detector generates data at ∼480 Gbit/s which is …
View article: Strain Field Around Individual Dislocations Controls Failure
Strain Field Around Individual Dislocations Controls Failure Open
Understanding material failure on a fundamental level is a key aspect in the design of robust structural materials, especially for metals and alloys capable to undergo plastic deformation. In the last decade, significant progress is made i…
View article: Atomic short-range order in SiGeSn alloys
Atomic short-range order in SiGeSn alloys Open
Neighborhood at atomic scale is important for the properties of advanced alloys. The preference or avoidance between neighboring atomic species is known as chemical short-range order (SRO). While SRO in metallic medium/high entropy alloys …
View article: Degradation of the mechanical properties of NbMoTaW refractory high-entropy alloy in tension
Degradation of the mechanical properties of NbMoTaW refractory high-entropy alloy in tension Open
View article: Multiple origins of extra electron diffractions in fcc metals
Multiple origins of extra electron diffractions in fcc metals Open
Diffuse intensities in the electron diffraction patterns of concentrated face-centered cubic solid solutions have been widely attributed to chemical short-range order, although this connection has been recently questioned. This article exp…
View article: Correlated 4D-STEM and EDS for the classification of fine Beta-precipitates in aluminum alloy AA 6063-T6
Correlated 4D-STEM and EDS for the classification of fine Beta-precipitates in aluminum alloy AA 6063-T6 Open
View article: Elucidating the role of Cr migration in Ni-Cr exposed to molten FLiNaK via multiscale characterization
Elucidating the role of Cr migration in Ni-Cr exposed to molten FLiNaK via multiscale characterization Open
Structural materials used in nuclear reactor environments are subjected to coupled extremes such as high temperature, irradiation, and corrosion which act in concert to degrade their functional performance. Connecting alloy microstructure …
View article: Morphological Evolution and Dealloying During Corrosion of Ni20Cr (wt.%) in Molten FLiNaK Salts
Morphological Evolution and Dealloying During Corrosion of Ni20Cr (wt.%) in Molten FLiNaK Salts Open
The dealloying corrosion behavior of the FCC Ni20Cr (wt%) in molten LiF-NaF-KF (FLiNaK) salts at 600 °C under varying applied potentials was investigated. Using in-operando electrochemical techniques and a multi-modal suite of characteriza…
View article: Light-driven C–H activation mediated by 2D transition metal dichalcogenides
Light-driven C–H activation mediated by 2D transition metal dichalcogenides Open
View article: MicroED-Informed 4D-STEM of MOFs for Carbon Capture
MicroED-Informed 4D-STEM of MOFs for Carbon Capture Open
View article: Charge-Induced Structural Rearrangements in Organic Mixed Ionic Electronic Conductors: A Cryogenic 4D-STEM Study
Charge-Induced Structural Rearrangements in Organic Mixed Ionic Electronic Conductors: A Cryogenic 4D-STEM Study Open
View article: Author Correction: Proton irradiation-decelerated intergranular corrosion of Ni-Cr alloys in molten salt
Author Correction: Proton irradiation-decelerated intergranular corrosion of Ni-Cr alloys in molten salt Open
View article: Tensile creep behavior of the Nb45Ta25Ti15Hf15 refractory high entropy alloy
Tensile creep behavior of the Nb45Ta25Ti15Hf15 refractory high entropy alloy Open