Arthur Edelmann
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View article: Synthesis and Crystal Structure of Rb[B(SO<sub>4</sub>)<sub>2</sub>]: A Borosulfate Obtained from a Reaction with Chlorosulfuric Acid
Synthesis and Crystal Structure of Rb[B(SO<sub>4</sub>)<sub>2</sub>]: A Borosulfate Obtained from a Reaction with Chlorosulfuric Acid Open
The solvothermal reaction of RbCl, boric acid, and chlorosulfuric acid yielded Rb[B(SO 4 ) 2 ]. The crystal structure of Rb[B(SO 4 ) 2 ] (tetragonal, P 4/ ncc, Z = 4, a = 9.1823(3) Å, c = 7.4559(5) Å, V = 628.64(6) Å) is isotypical to the …
View article: Cover Feature: Pd[B(S <sub>2</sub> O <sub>7</sub> ) <sub>2</sub> ] <sub>2</sub> and Pd[B(SO <sub>4</sub> ) (S <sub>2</sub> O <sub>7</sub> )] <sub>2</sub> : Two Borosulfates with Pd <sup>2+</sup> in Octahedral and One with Pd <sup>2+</sup> in Square Planar Oxygen Coordination
Cover Feature: Pd[B(S <sub>2</sub> O <sub>7</sub> ) <sub>2</sub> ] <sub>2</sub> and Pd[B(SO <sub>4</sub> ) (S <sub>2</sub> O <sub>7</sub> )] <sub>2</sub> : Two Borosulfates with Pd <sup>2+</sup> in Octahedral and One with Pd <sup>2+</sup> in Square Planar Oxygen Coordination Open
View article: Pd[B(S <sub>2</sub> O <sub>7</sub> ) <sub>2</sub> ] <sub>2</sub> and Pd[B(SO <sub>4</sub> ) (S <sub>2</sub> O <sub>7</sub> )] <sub>2</sub> : Two Borosulfates with Pd <sup>2+</sup> in Octahedral and One with Pd <sup>2+</sup> in Square Planar Oxygen Coordination
Pd[B(S <sub>2</sub> O <sub>7</sub> ) <sub>2</sub> ] <sub>2</sub> and Pd[B(SO <sub>4</sub> ) (S <sub>2</sub> O <sub>7</sub> )] <sub>2</sub> : Two Borosulfates with Pd <sup>2+</sup> in Octahedral and One with Pd <sup>2+</sup> in Square Planar Oxygen Coordination Open
The reaction of elemental palladium with B 2 O 3 and SO 3 at elevated temperature results in the formation of blue crystals of Pd[B(S 2 O 7 ) 2 ] 2 . Dependent on the reaction conditions, the compound crystallizes in two different polymorp…