Bernd Hinrichsen
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View article: A reference material for X-ray diffraction line profile analysis
A reference material for X-ray diffraction line profile analysis Open
A nanocrystalline Fe–1.8%Cr steel powder was tested as a reference material on more than five powder diffraction instruments and configurations, as well as with different data-analysis methodologies. The material, commercially available at…
View article: Building a community lightsource meta-infrastructure to accelerate battery innovation in Europe
Building a community lightsource meta-infrastructure to accelerate battery innovation in Europe Open
Breakthroughs in battery research are imperative to provide society with batteries that are safe and sustainable, have a high energy density, and have a long cycle life at low cost. Recent advances in research methodologies, the emergence …
View article: Multimodal Hard X‐Ray Nanotomography Probes Pore Accessibility of Technical Catalysts after Coking
Multimodal Hard X‐Ray Nanotomography Probes Pore Accessibility of Technical Catalysts after Coking Open
Coking is a common catalyst deactivation route in industrial processes involving carbonaceous species. While coking is easy to diagnose, this is often performed by bulk analysis. Understanding specific symptoms such as pore blockage and ob…
View article: Quantifying the cooperative evolution of microphase segregation and nanostructural order in annealed polyurethanes of <scp>MDI‐BDO‐PTHF</scp>
Quantifying the cooperative evolution of microphase segregation and nanostructural order in annealed polyurethanes of <span>MDI‐BDO‐PTHF</span> Open
Here, we quantify the relationship between microphase segregation and local structure development in thermoplastic polyurethanes. Samples were prepared with varying ratios of 4,4′‐methylene diphenyl diisocyanate (MDI) and 1,4‐butanediol (B…
View article: Adapting the European Synchrotron to Industry
Adapting the European Synchrotron to Industry Open
International audience
View article: Architecture of industrial Bi-Mo-Co-Fe-K-O propene oxidation catalysts
Architecture of industrial Bi-Mo-Co-Fe-K-O propene oxidation catalysts Open
Industrial heterogeneous catalysts show high performance coupled with high material complexity. Deconvoluting this complexity into simplified models eases mechanistic studies. However, this approach dilutes the relevance because models are…
View article: A previously unknown cyclic alkanolamine and molecular ranking using the pair distribution function
A previously unknown cyclic alkanolamine and molecular ranking using the pair distribution function Open
A new six-membered cyclic alkanolamine with chemical formula C 6 H 15 N 3 O 3 was synthesized by the reaction of glycolaldehyde with gaseous ammonia. The molecular structure, characterized by a hexagonal ring of alternating carbon and nitr…
View article: Cross-examining Polyurethane Nanodomain Formation and Internal Structure
Cross-examining Polyurethane Nanodomain Formation and Internal Structure Open
Structural and morphological interplay between hard and soft phases determine the bulk properties of thermoplastic polyurethanes. Commonly employed techniques rely on different physical or chemical phenomena for characterizing the organiza…
View article: Improving the picture of atomic structure in nonoriented polymer domains using the pair distribution function: A study of polyamide 6
Improving the picture of atomic structure in nonoriented polymer domains using the pair distribution function: A study of polyamide 6 Open
Investigations of the atomic structures within polyamides started over 80 years ago and continue today. These weakly ordered materials diffract X‐rays poorly and typically require postprocessing to obtain idealized samples for structural s…
View article: A routine for the determination of the microstructure of stacking-faulted nickel cobalt aluminium hydroxide precursors for lithium nickel cobalt aluminium oxide battery materials
A routine for the determination of the microstructure of stacking-faulted nickel cobalt aluminium hydroxide precursors for lithium nickel cobalt aluminium oxide battery materials Open
The microstructures of six stacking-faulted industrially produced cobalt- and aluminium-bearing nickel layered double hydroxide (LDH) samples that are used as precursors for Li(Ni 1− x −y Co x Al y )O 2 battery materials were investigated.…
View article: CCDC 1560870: Experimental Crystal Structure Determination
CCDC 1560870: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 1560869: Experimental Crystal Structure Determination
CCDC 1560869: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: Crystallography in the globe's largest chemical company
Crystallography in the globe's largest chemical company Open
Research and development are the main drivers for growth in the chemical industry.Whereas large commodity products have low margins and are efficiency driven, specialized products can return larger profits to the company.It is the latter o…
View article: On Two Glycine Zinc Sulfate Phases with Exotic Cation Coordination Geometries
On Two Glycine Zinc Sulfate Phases with Exotic Cation Coordination Geometries Open
Two hitherto hardly characterized glycine zinc sulfates were identified in the product of a batch production process for glycine zinc sulfates of the BASF Company: Gly · ZnSO 4 · 2H 2 O and β‐Gly‐ZnSO 4 . The crystal structures were solved…
View article: CCDC 1481326: Experimental Crystal Structure Determination
CCDC 1481326: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 1481327: Experimental Crystal Structure Determination
CCDC 1481327: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 1481328: Experimental Crystal Structure Determination
CCDC 1481328: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 1481325: Experimental Crystal Structure Determination
CCDC 1481325: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …