Brian Perdue
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View article: Classification of commercial inorganic acids used in vitriolage from fibres analysis via FTIR-PCA
Classification of commercial inorganic acids used in vitriolage from fibres analysis via FTIR-PCA Open
Vitriolage (often referred to as 'acid attack') is a heinous crime with reported instances becoming more common, yet, literature precedence for elucidation of information pertinent to assisting vitriolage investigation is still scarce. In …
View article: Investigating safety in high nickel NMC||LTO Batteries
Investigating safety in high nickel NMC||LTO Batteries Open
View article: Interfacing durable materials to enable structural electronics
Interfacing durable materials to enable structural electronics Open
View article: Discharge in Unactivated Thermal Batteries
Discharge in Unactivated Thermal Batteries Open
View article: Effects of Applied Interfacial Pressure on Li-Metal Cycling Performance and Morphology in 4 M LiFSI in DME
Effects of Applied Interfacial Pressure on Li-Metal Cycling Performance and Morphology in 4 M LiFSI in DME Open
Lithium-metal anodes can theoretically enable 10× higher gravimetric capacity than conventional graphite anodes. However, Li-metal anode cycling has proven difficult due to porous and dendritic morphologies, extensive parasitic solid elect…
View article: The Effects of Applied Interfacial Pressure on Lithium Metal Cycling Behavior.
The Effects of Applied Interfacial Pressure on Lithium Metal Cycling Behavior. Open
ion beam milling and cryo-scanning electron microscopy imaging in cross section reveal that increasing the applied pressure during Li deposition from 0 to 10 MPa leads to greater than a fivefold reduction in thickness (and therefore volume…
View article: Use of a beryllium-dome holder for texture and strain characterization of Li metal thin films via Tilt-A-Whirl methodology.
Use of a beryllium-dome holder for texture and strain characterization of Li metal thin films via Tilt-A-Whirl methodology. Open
View article: The Effects of Applied Interfacial Compression on Lithium Metal Cycling Behavior.
The Effects of Applied Interfacial Compression on Lithium Metal Cycling Behavior. Open
ion beam milling and cryo-scanning electron microscopy imaging in cross section reveal that increasing the applied pressure during Li deposition from 0 to 10 MPa leads to greater than a fivefold reduction in thickness (and therefore volume…
View article: 8-1-19 Weekly Update SNL Testing.
8-1-19 Weekly Update SNL Testing. Open
View article: Use of a Be-dome holder for texture and strain characterization of Li metal thin films via sin<sup>2</sup>(<i>ψ</i>) methodology
Use of a Be-dome holder for texture and strain characterization of Li metal thin films via sin<sup>2</sup>(<i>ψ</i>) methodology Open
Residual strain in electrodeposited Li films may affect safety and performance in Li metal battery anodes, so it is important to understand how to detect residual strain in electrodeposited Li and the conditions under which it arises. To e…
View article: Testing Update SNL (Q2 FY2020)
Testing Update SNL (Q2 FY2020) Open
Two different cell constructions are currently being investigated for the LFP/Graphite system. These cells have undergone continuous cycling until the target of 1000 cycles was reached.
View article: SEM, TEM, and Cryo-EM of Electrodeposited Li, Mg, and Ca Metal Electrodes
SEM, TEM, and Cryo-EM of Electrodeposited Li, Mg, and Ca Metal Electrodes Open
Journal Article SEM, TEM, and Cryo-EM of Electrodeposited Li, Mg, and Ca Metal Electrodes Get access Katherine Jungjohann, Katherine Jungjohann Center for Integrated Nanotechnologies, Sandia National Laboratories, Albuquerque, USA Correspo…
View article: BTMS Testing Section
BTMS Testing Section Open
Cell testing is an important part of understanding the performance and life capabilities of state-of-the art energy storage technologies, particularly with respect to the distinct technical and functional requirements posed by the BTMS pro…
View article: Carbon Monofluoride Based High Voltage Thermal Battery Cathode.
Carbon Monofluoride Based High Voltage Thermal Battery Cathode. Open
View article: Nanoporous Polymer Films with a High Cation Transference Number Stabilize Lithium Metal Anodes in Light-Weight Batteries for Electrified Transportation
Nanoporous Polymer Films with a High Cation Transference Number Stabilize Lithium Metal Anodes in Light-Weight Batteries for Electrified Transportation Open
To suppress dendrite formation in lithium metal batteries, high cation transference number electrolytes that reduce electrode polarization are highly desirable, but rarely available using conventional liquid electrolytes. Here, we show tha…
View article: Using X-ray Spectromicroscopy for Operando Characterization of Li-S Batteries
Using X-ray Spectromicroscopy for Operando Characterization of Li-S Batteries Open
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View article: Polysulfide Speciation in the Bulk Electrolyte of a Lithium Sulfur Battery
Polysulfide Speciation in the Bulk Electrolyte of a Lithium Sulfur Battery Open
In situ Raman microscopy was used to study polysulfide speciation in the bulk ether electrolyte during the discharge and charge of a Li-S electrochemical cell to assess the complex interplay between chemical and electrochemical reactions i…
View article: Operando Spectromicroscopy of Sulfur Species in Lithium-Sulfur Batteries
Operando Spectromicroscopy of Sulfur Species in Lithium-Sulfur Batteries Open
Here, a novel cross-sectional battery cell was developed to characterize lithium-sulfur batteries using X-ray spectromicroscopy. Chemically sensitive X-ray maps were collected operando at energies relevant to the expected sulfur species an…
View article: The effect of water-containing electrolyte on lithium-sulfur batteries
The effect of water-containing electrolyte on lithium-sulfur batteries Open
View article: Concept Integration and Scale Up for Demonstrating Li-S.
Concept Integration and Scale Up for Demonstrating Li-S. Open
View article: Systematic Variation of Sulfur Cathode Chemistry and its Effects on Cell Performance.
Systematic Variation of Sulfur Cathode Chemistry and its Effects on Cell Performance. Open
View article: Electrolyte-Binder Powder Processing to Improve Manufacturability of Thermal Battery Separator Pellets.
Electrolyte-Binder Powder Processing to Improve Manufacturability of Thermal Battery Separator Pellets. Open
View article: Electrochemical Formation of Germanene: pH 4.5
Electrochemical Formation of Germanene: pH 4.5 Open
Germanene is a single layer allotrope of Ge, with a honeycomb structure similar to graphene. This report concerns the electrochemical formation of germanene in a pH 4.5 solution. The studies were performed using in situ Electrochemical Sca…
View article: Performance of a MgS battery using Grignard Based Electrolytes.
Performance of a MgS battery using Grignard Based Electrolytes. Open
View article: LiS Pouch Cell Fabrication and Cathode Prototyping.
LiS Pouch Cell Fabrication and Cathode Prototyping. Open
View article: Nanoporous-Carbon as a Potential Host Material for Reversible Mg Ion Intercalation
Nanoporous-Carbon as a Potential Host Material for Reversible Mg Ion Intercalation Open
Here, we study nanoporous-carbon (NPC) grown via pulsed laser deposition (PLD) as an electrically conductive anode host material for Mg2+ intercalation. NPC has high surface area, and an open, accessible pore structure tunable v…
View article: Understanding Performance Limitations to Enable High Performance Magnesium-Ion Batteries
Understanding Performance Limitations to Enable High Performance Magnesium-Ion Batteries Open
We developed a mathematical model in order to investigate the performance limiting factors of Mg-ion battery with a Chevrel phase (MgxMo6S8) cathode and a Mg metal anode. Furthermore, the model was validate…