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View article: Kinetics study of the dissolution of black mass material using oxalic acid as a leaching agent
Kinetics study of the dissolution of black mass material using oxalic acid as a leaching agent Open
This study investigates the dissolution mechanisms of black mass by employing oxalic acid as a leaching agent at different temperatures. The concentration of oxalic acid and the solid-to-liquid ratio of the leaching are maintained at a fix…
View article: Exploring the Solubility of Ethylene Carbonate in Supercritical Carbon Dioxide: A Pathway for Sustainable Electrolyte Recycling from Li-Ion Batteries
Exploring the Solubility of Ethylene Carbonate in Supercritical Carbon Dioxide: A Pathway for Sustainable Electrolyte Recycling from Li-Ion Batteries Open
Ethylene carbonate is, among other applications, used in Li-ion batteries as an electrolyte solvent to dissociate Li-salt. Supercritical CO2 extraction is a promising method for the recycling of electrolyte solvents from spent batteries. T…
View article: A Simple Step-by-Step Guide to the Design and Analysis of Unreplicated Split-Plot Experiments Through a Case Study on Molybdenum Recycling from CIGS Solar Cells
A Simple Step-by-Step Guide to the Design and Analysis of Unreplicated Split-Plot Experiments Through a Case Study on Molybdenum Recycling from CIGS Solar Cells Open
Considerable effort has been put over the last few decades into clarifying the correct design and analysis of split-plot factorial experiments. However, the information found in the literature is scattered and sometimes still not easy to g…
View article: Production of High Purity MnSO <sub>4</sub> ·H <sub>2</sub> O from Real NMC111 Lithium-Ion Batteries Leachate Using Solvent Extraction and Evaporative Crystallization
Production of High Purity MnSO <sub>4</sub> ·H <sub>2</sub> O from Real NMC111 Lithium-Ion Batteries Leachate Using Solvent Extraction and Evaporative Crystallization Open
Recovery of manganese as high purity MnSO4·H2O from purified NMC111 lithium-ion battery leachate using solvent extraction and evaporative crystallization was investigated. Bis(2-ethylhexyl) phosphoric acid (D2EHPA) was used for Mn extracti…
View article: Resource Recovery of Spent Lithium-Ion Battery Cathode Materials by a Supercritical Carbon Dioxide System
Resource Recovery of Spent Lithium-Ion Battery Cathode Materials by a Supercritical Carbon Dioxide System Open
The increasing global market size of high-energy storage devices due to the boom in electric vehicles and portable electronics has caused the battery industry to produce a lot of waste lithium-ion batteries. The liberation and de-agglomera…
View article: An environmentally friendly method for selective recovery of silver and ITO particles from flexible CIGS solar cells
An environmentally friendly method for selective recovery of silver and ITO particles from flexible CIGS solar cells Open
While the share of solar energy harvesting by photovoltaic (PV) systems in electricity production increases, their recycling still remains mainly at an early stage. Therefore, valuable and critical elements like silver (Ag) and indium (In)…
View article: Disordered Crystal Structure and Anomalously High Solubility of Radium Carbonate
Disordered Crystal Structure and Anomalously High Solubility of Radium Carbonate Open
Radium-226 carbonate was synthesized from radium-barium sulfate (226Ra0.76Ba0.24SO4) at room temperature and characterized by X-ray powder diffraction (XRPD) and extended X-ray absorption fine structure (EXAFS) techniques. XRPD revealed th…
View article: Valuable metal recycling from thin film CIGS solar cells by leaching under mild conditions
Valuable metal recycling from thin film CIGS solar cells by leaching under mild conditions Open
The increase in the manufacturing of copper-indium-gallium-diselenide (CIGS) thin film photovoltaics is accompanied by a growing amount of production waste, which contains a mixture of valuable, critical and hazardous elements. However, in…
View article: Electrolyte recovery from spent Lithium-Ion batteries using a low temperature thermal treatment process
Electrolyte recovery from spent Lithium-Ion batteries using a low temperature thermal treatment process Open
Electrolyte recovery is seldomly considered in state-of-art lithium-ion battery recycling methods but rather evaporates and decomposes uncontrolled during the pre-treatment steps. However, controlled and safe removal of the electrolyte is …
View article: Mixed Oxides NiO/ZnO/Al2O3 Synthesized in a Single Step via Ultrasonic Spray Pyrolysis (USP) Method
Mixed Oxides NiO/ZnO/Al2O3 Synthesized in a Single Step via Ultrasonic Spray Pyrolysis (USP) Method Open
Mixed oxides have received remarkable attention due to the many opportunities to adjust their interesting structural, electrical, catalytic properties, leading to a better, more useful performance compared to the basic metal oxides. In thi…
View article: Recovery of critical metals from EV batteries via thermal treatment and leaching with sulphuric acid at ambient temperature
Recovery of critical metals from EV batteries via thermal treatment and leaching with sulphuric acid at ambient temperature Open
In the upcoming years, todaýs e-mobility will challenge the capacity of sustainable recycling. Due to the presence of organic components (electrolyte, separator, casings, etc.), future recycling technologies will combine thermal pre-treatm…
View article: One Step Production of Silver-Copper (AgCu) Nanoparticles
One Step Production of Silver-Copper (AgCu) Nanoparticles Open
AgCu nanoparticles were prepared through hydrogen-reduction-assisted Ultrasonic Spray Pyrolysis (USP) and the Hydrogen Reduction (HR) method. The changes in the morphology and crystal structure of nanoparticles were studied using different…
View article: Investigation of indium and other valuable metals leaching from unground waste LCD screens by organic and inorganic acid leaching
Investigation of indium and other valuable metals leaching from unground waste LCD screens by organic and inorganic acid leaching Open
Indium (In) is the indispensable part of liquid crystal display (LCD) screen which is applied as a thin semiconductor layer on the surface mainly in the form of indium tin oxide (ITO), and feasible end-of-life recycling of indium from this…
View article: Innovative recycling of organic binders from electric vehicle lithium-ion batteries by supercritical carbon dioxide extraction
Innovative recycling of organic binders from electric vehicle lithium-ion batteries by supercritical carbon dioxide extraction Open
The growing demand for energy storage devices due to the skyrocketing production/consumption of portable electrical and electronic equipment as well as electric vehicles has promoted battery technologies, resulting in the piling of a large…
View article: Hydrometallurgical recycling of EV lithium-ion batteries: Effects of incineration on the leaching efficiency of metals using sulfuric acid
Hydrometallurgical recycling of EV lithium-ion batteries: Effects of incineration on the leaching efficiency of metals using sulfuric acid Open
The growing demand for lithium-ion batteries will result in an increasing flow of spent batteries, which must be recycled to prevent environmental and health problems, while helping to mitigate the raw materials dependence and risks of sho…
View article: Waste of batteries management: Synthesis of magnetocaloric manganite compound from the REEs mixture generated during hydrometallurgical processing of NiMH batteries
Waste of batteries management: Synthesis of magnetocaloric manganite compound from the REEs mixture generated during hydrometallurgical processing of NiMH batteries Open
In the present study, rare earth elements (REEs, i.e., La, Ce, Nd, and Pr) were hydrometallurgically recovered in oxalate form with presence of very low concentration of Co, Al, Zn and Ni from solution after processing of spent Nickel meta…
View article: Comparison of the effects of incineration, vacuum pyrolysis and dynamic pyrolysis on the composition of NMC-lithium battery cathode-material production scraps and separation of the current collector
Comparison of the effects of incineration, vacuum pyrolysis and dynamic pyrolysis on the composition of NMC-lithium battery cathode-material production scraps and separation of the current collector Open
The rising demand for lithium batteries is challenging battery producers to increase their production. This is causing an accumulation of production scrap which must be treated to allow re-utilization of cathode material in production. Sev…
View article: Considerations when Modelling EV Battery Circularity Systems
Considerations when Modelling EV Battery Circularity Systems Open
The electric vehicle market is expected to grow substantially in the coming years, which puts new requirements on the end-of-life phase and on the recycling systems. To a larger extent, the environmental footprint from these vehicles is re…
View article: Simple Preparation of Ni and NiO Nanoparticles Using Raffinate Solution Originated from Spent NiMH Battery Recycling
Simple Preparation of Ni and NiO Nanoparticles Using Raffinate Solution Originated from Spent NiMH Battery Recycling Open
Nickel (Ni) and nickel oxide (NiO) nanoparticles were produced by a combination of precipitation and reduction/calcination methods using the raffinate solution originated from laboratory scale spent NiMH recovery process. Ni recovery from …
View article: Physical separation, mechanical enrichment and recycling-oriented characterization of spent NiMH batteries
Physical separation, mechanical enrichment and recycling-oriented characterization of spent NiMH batteries Open
Nickel–metal hydride (NiMH) batteries contain high amount of industrial metals, especially iron, nickel, cobalt and rare earth elements. Although the battery waste is a considerable secondary source for metal and chemical industries, a rec…