Xiaodong Zou
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View article: Serial Chemical Crystallography for Autonomous Quantitative Phase Analysis in an Electron Microscope
Serial Chemical Crystallography for Autonomous Quantitative Phase Analysis in an Electron Microscope Open
We present serial electron diffraction with tilt (t‐SerialED), a method for fast autonomous phase and structural analysis of beam‐sensitive, nano‐sized polycrystalline materials. Unlike traditional workflows collecting datasets crystal by …
View article: Automated and real-time structure solution using 3D electron diffraction
Automated and real-time structure solution using 3D electron diffraction Open
Three-dimensional electron diffraction (3D ED) has emerged as a powerful tool for solving the structures of small crystals down to nanometre-scale sizes. Despite advancements in automating data acquisition for 3D ED, the subsequent data pr…
View article: Efficacy and safety of traditional Chinese medicine combined with immunomodulators in treating erosive oral lichen planus: A network meta-analysis of randomized controlled trials
Efficacy and safety of traditional Chinese medicine combined with immunomodulators in treating erosive oral lichen planus: A network meta-analysis of randomized controlled trials Open
Background: This study aimed to systematically evaluate the efficacy and safety of various Chinese herbal medicines combined with immunomodulators (IMM) in the treatment of erosive oral lichen planus (EOLP) through a network meta-analysis.…
View article: Continuous Serial Electron Diffraction for High Quality Protein Structures
Continuous Serial Electron Diffraction for High Quality Protein Structures Open
Determining macromolecular structures is crucial for understanding biological mechanisms and advancing drug discovery. Three-dimensional electron diffraction (3D ED), also known as microcrystal electron diffraction (MicroED) using continuo…
View article: Einblicke in die Kohlenmonoxid‐Reduktionsreaktion auf Cu(111) durch elektrochemische <i>Operando</i> Röntgen‐Photoelektronenspektroskopie
Einblicke in die Kohlenmonoxid‐Reduktionsreaktion auf Cu(111) durch elektrochemische <i>Operando</i> Röntgen‐Photoelektronenspektroskopie Open
Abstrakt In dieser Arbeit stellen wir einen modifizierten Ansatz der elektrochemischen Röntgen‐Photoelektronenspektroskopie (ECXPS) vor, der neue mechanistische Einblicke in die alkalische Kohlenmonoxid‐Reduktionsreaktion (CORR) an einer C…
View article: Insight into the Carbon Monoxide Reduction Reaction on Cu(111) from <i>Operando</i> Electrochemical X‐ray Photoelectron Spectroscopy
Insight into the Carbon Monoxide Reduction Reaction on Cu(111) from <i>Operando</i> Electrochemical X‐ray Photoelectron Spectroscopy Open
In this work, we introduce a modified dip‐and‐pull electrochemical X‐ray photoelectron spectroscopy (ECXPS) approach that offers new mechanistic insight into the alkaline carbon monoxide reduction reaction (CORR) over a Cu(111) single crys…
View article: Unveiling the Structure of Anhydrous Sodium Valproate with 3D Electron Diffraction and a Facile Sample Preparation Workflow
Unveiling the Structure of Anhydrous Sodium Valproate with 3D Electron Diffraction and a Facile Sample Preparation Workflow Open
Understanding the structure of an active pharmaceutical ingredient is essential for gaining insights into its physicochemical properties. Sodium valproate, one of the most effective antiepileptic drugs, was first approved for medical use i…
View article: AutoLEI: An XDS-based Graphical User Interface for Automated Real-time and Offline Batch 3D ED/MicroED Data Processing
AutoLEI: An XDS-based Graphical User Interface for Automated Real-time and Offline Batch 3D ED/MicroED Data Processing Open
Three-dimensional electron diffraction (3D ED), also known as microcrystal electron diffraction (MicroED), is an emerging method for determining structures of submicron-sized crystals. With the development of rapid and convenient data coll…
View article: Automated and real-time structure solution using 3D electron diffraction
Automated and real-time structure solution using 3D electron diffraction Open
Three-dimensional electron diffraction (3D ED) has emerged as a powerful tool for solving the structures of small crystals down to nanometre-scale sizes. Despite advancements in automating data acquisition for 3D ED, the subsequent data pr…
View article: Morphological Comparison Between Two Model Groups of the Same Product Family Belonging to Different Price Levels
Morphological Comparison Between Two Model Groups of the Same Product Family Belonging to Different Price Levels Open
View article: Insight into the carbon monoxide reduction reaction on Cu(111) from operando electrochemical X-ray photoelectron spectroscopy
Insight into the carbon monoxide reduction reaction on Cu(111) from operando electrochemical X-ray photoelectron spectroscopy Open
In this work, we introduce a modified dip-and-pull ECXPS approach that offers new mechanistic insight into the alkaline CORR over a Cu(111) single crystal surface. We tackle two major unresolved questions in the CORR mechanism that persist…
View article: Atomic-scale insights into topotactic transformations in an extra-large-pore zeolite using time-resolved 3D electron diffraction
Atomic-scale insights into topotactic transformations in an extra-large-pore zeolite using time-resolved 3D electron diffraction Open
Understanding the atomic-scale structural dynamics of phase transformations is crucial for developing materials and tailoring their properties. However, many materials are obtained as polycrystalline powders with large unit cells and/or co…
View article: A stable zeolite with atomically ordered and interconnected mesopore channel
A stable zeolite with atomically ordered and interconnected mesopore channel Open
View article: Localized Boron Sites in Large Pore Borosilicate Zeolite EMM-59 Determined by Electron Crystallography
Localized Boron Sites in Large Pore Borosilicate Zeolite EMM-59 Determined by Electron Crystallography Open
The structure of novel large pore borosilicate zeolite EMM-59 (|C19H42N2|8[B5.2Si218.8O448]) with localized framework boron sites was determined by using three-di…
View article: How to use <i>DIALS</i> to process chemical crystallography 3D ED rotation data from pixel array detectors
How to use <i>DIALS</i> to process chemical crystallography 3D ED rotation data from pixel array detectors Open
The DIALS package provides a set of tools for crystallographic data processing. The open-source nature of the project, and a flexible interface in which individual command-line programs each have a dedicated job, have enabled the adaptatio…
View article: Research on robust control strategies for diesel engines based on H∞ theory
Research on robust control strategies for diesel engines based on H∞ theory Open
View article: Serial chemical crystallography for autonomous quantitative phase analysis in an electron microscope
Serial chemical crystallography for autonomous quantitative phase analysis in an electron microscope Open
Recent advancements in robotics and artificial intelligence have accelerated the development of autonomous workflows for material discovery. Powder X-ray diffraction (PXRD) remains the primary method for characterizing crystal structures i…
View article: Localized Boron Sites in Large Pore Borosilicate Zeolite EMM-59 Determined by Electron Crystallography
Localized Boron Sites in Large Pore Borosilicate Zeolite EMM-59 Determined by Electron Crystallography Open
The structure of a novel large pore borosilicate zeolite EMM-59 (|C19H42N2|8[B5.2Si218.8O448]) with localized framework boron sites was determined using three-dimensional electron diffraction (3D ED) and scanning transmission electron micr…
View article: Development of PIND system based on resonant sensors and research on material identification methods for redundant particles
Development of PIND system based on resonant sensors and research on material identification methods for redundant particles Open
Aiming at the problems of the existing particle impact noise detection (PIND) system, such as low detection accuracy, high rate of misjudgment and missed judgment, and the inability to judge the material of internal redundant particles in …
View article: On the structure refinement of metal complexes against 3D electron diffraction data using multipolar scattering factors
On the structure refinement of metal complexes against 3D electron diffraction data using multipolar scattering factors Open
This study examines various methods for modelling the electron density and, thus, the electrostatic potential of an organometallic complex for use in crystal structure refinement against 3D electron diffraction (ED) data. It focuses on mod…
View article: Atomic-scale insights into topotactic transformations in extra-large pore silicate zeolites using time-resolved 3D electron diffraction
Atomic-scale insights into topotactic transformations in extra-large pore silicate zeolites using time-resolved 3D electron diffraction Open
Understanding the atomic scale structural dynamics of phase transformations is crucial for developing new materials and tailoring the properties of the materials. However, many materials are obtained as polycrystalline powders with large u…
View article: Phase Identification and Discovery of an Elusive Polymorph of Drug‐Polymer Inclusion Complex Using Automated 3D Electron Diffraction
Phase Identification and Discovery of an Elusive Polymorph of Drug‐Polymer Inclusion Complex Using Automated 3D Electron Diffraction Open
3D electron diffraction (3D ED) has shown great potential in crystal structure determination in materials, small organic molecules, and macromolecules. In this work, an automated, low‐dose and low‐bias 3D ED protocol has been implemented t…
View article: Atomic-scale insights into topotactic transformations in extra-large pore silicate zeolites using time-resolved 3D electron diffraction
Atomic-scale insights into topotactic transformations in extra-large pore silicate zeolites using time-resolved 3D electron diffraction Open
Understanding the atomic scale structural dynamics of phase transformations is crucial for developing new materials and tailoring the properties of the materials. However, many materials are obtained as polycrystalline powders with large u…
View article: Confined single-molecule imaging by low-dose electron microscopy
Confined single-molecule imaging by low-dose electron microscopy Open
View article: Discovery of Novel Nanoporous Materials Advanced by Electron Crystallography
Discovery of Novel Nanoporous Materials Advanced by Electron Crystallography Open
View article: Visualizing atomic structure of novel three-dimensional covalent organic frameworks by 3DED and high-resolution (S)TEM
Visualizing atomic structure of novel three-dimensional covalent organic frameworks by 3DED and high-resolution (S)TEM Open
View article: Insights on the disordered nature in amorphous-based anode materials from Electron Pair Distribution Function
Insights on the disordered nature in amorphous-based anode materials from Electron Pair Distribution Function Open
View article: STEM SerialED: achieving high-resolution data for <i>ab initio</i> structure determination of beam-sensitive nanocrystalline materials
STEM SerialED: achieving high-resolution data for <i>ab initio</i> structure determination of beam-sensitive nanocrystalline materials Open
Serial electron diffraction (SerialED), which applies a snapshot data acquisition strategy for each crystal, was introduced to tackle the problem of radiation damage in the structure determination of beam-sensitive materials by three-dimen…
View article: STEM SerialED: achieving high-resolution data for ab initio structure determination of beam-sensitive nanocrystalline materials
STEM SerialED: achieving high-resolution data for ab initio structure determination of beam-sensitive nanocrystalline materials Open
Serial electron diffraction (SerialED), which applies a snapshot data acquisition strategy on each crystal, was introduced to tackle the problem of radiation damage in the structure determination of beam-sensitive materials by three-dimens…
View article: Visualization of topotactic structural transformations of zeolites using 3D electron diffraction
Visualization of topotactic structural transformations of zeolites using 3D electron diffraction Open
Knowing the structures of intermediates in phase transformations is crucial for elucidating the formation mechanisms and tailoring the properties of many industrially important materials, ranging from ceramics1 alloys/metal oxides2-5and ba…