Hellmut Eckert
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View article: Polar covalent apex‐base bonding in borapyramidanes probed by solid‐state NMR and DFT calculations
Polar covalent apex‐base bonding in borapyramidanes probed by solid‐state NMR and DFT calculations Open
Pyramidane molecules have attracted chemists for many decades due to their regular shape, high symmetry and their correspondence in the macroscopic world. Recently, experimental access to a number of examples has been reported, in particul…
View article: Extending the Palette of Luminescent Primary Thermometers: Yb<sup>3+</sup>/Pr<sup>3+</sup> Co-Doped Fluoride Phosphate Glasses
Extending the Palette of Luminescent Primary Thermometers: Yb<sup>3+</sup>/Pr<sup>3+</sup> Co-Doped Fluoride Phosphate Glasses Open
The unique tunable properties of glasses make them versatile materials for developing numerous state-of-the-art optical technologies. To design new optical glasses with tailored properties, an extensive understanding of the intricate corre…
View article: Structure of amorphous materials in the NASICON system Na 1+x Ti<sub>2</sub>Si<sub> x </sub>P 3−x O<sub>12</sub>
Structure of amorphous materials in the NASICON system Na 1+x Ti<sub>2</sub>Si<sub> x </sub>P 3−x O<sub>12</sub> Open
The structure of glasses in the sodium (Na) super-ionic conductor (NASICON) system Na Ti 2 Si x P O 12 with x = 0.8 and x = 1.0 was explored by combining neutron and high-energy x-ray diffraction with 29 Si, 31 P and 23 Na sol…
View article: Structure of diopside, enstatite, and magnesium aluminosilicate glasses: A joint approach using neutron and x-ray diffraction and solid-state NMR
Structure of diopside, enstatite, and magnesium aluminosilicate glasses: A joint approach using neutron and x-ray diffraction and solid-state NMR Open
Neutron diffraction with magnesium isotope substitution, high energy x-ray diffraction, and 29Si, 27Al, and 25Mg solid-state nuclear magnetic resonance (NMR) spectroscopy were used to measure the structure of glassy diopside (CaMgSi2O6), e…
View article: CCDC 2181424: Experimental Crystal Structure Determination
CCDC 2181424: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2181414: Experimental Crystal Structure Determination
CCDC 2181414: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2181416: Experimental Crystal Structure Determination
CCDC 2181416: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2181423: Experimental Crystal Structure Determination
CCDC 2181423: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2181415: Experimental Crystal Structure Determination
CCDC 2181415: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2181421: Experimental Crystal Structure Determination
CCDC 2181421: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2181420: Experimental Crystal Structure Determination
CCDC 2181420: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2181418: Experimental Crystal Structure Determination
CCDC 2181418: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2181417: Experimental Crystal Structure Determination
CCDC 2181417: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2181419: Experimental Crystal Structure Determination
CCDC 2181419: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2181422: Experimental Crystal Structure Determination
CCDC 2181422: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: Oxy‐Borylenes as Photoreductants: Synthesis and Application in Dehalogenation and Detosylation Reactions
Oxy‐Borylenes as Photoreductants: Synthesis and Application in Dehalogenation and Detosylation Reactions Open
While the range of accessible borylenes has significantly broadened over the last decade, applications remain limited. Herein, we present tricoordinate oxy‐borylenes as potent photoreductants that can be readily activated by visible light.…
View article: Solid‐state NMR investigation of fast sodium ion‐conducting glass–ceramics: The system Na <sub>3+3</sub> <i> <sub>x</sub> </i> <sub>−</sub> <i> <sub>y</sub> </i> RE <sub>1−</sub> <i> <sub>x</sub> </i> P <i> <sub>y</sub> </i> Si <sub>3−</sub> <i> <sub>y</sub> </i> O <sub>9</sub> (RE = Sc, Y)
Solid‐state NMR investigation of fast sodium ion‐conducting glass–ceramics: The system Na <sub>3+3</sub> <i> <sub>x</sub> </i> <sub>−</sub> <i> <sub>y</sub> </i> RE <sub>1−</sub> <i> <sub>x</sub> </i> P <i> <sub>y</sub> </i> Si <sub>3−</sub> <i> <sub>y</sub> </i> O <sub>9</sub> (RE = Sc, Y) Open
Glasses and glass–ceramics of composition Na 3+3 x − y RE 1− x P y Si 3− y O 9 were synthesized using RE = Sc and Y, x = 0.4, and y = 0.0 and 0.3 to obtain multiple‐phase glass–ceramics containing the highly conducting Na 5 RESi 4 O 12 (N5…
View article: CSD 1791571: Experimental Crystal Structure Determination
CSD 1791571: Experimental Crystal Structure Determination Open
An entry from the Inorganic Crystal Structure Database, the world’s repository for inorganic crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely availabl…
View article: CSD 1791569: Experimental Crystal Structure Determination
CSD 1791569: Experimental Crystal Structure Determination Open
An entry from the Inorganic Crystal Structure Database, the world’s repository for inorganic crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely availabl…
View article: CSD 1791567: Experimental Crystal Structure Determination
CSD 1791567: Experimental Crystal Structure Determination Open
An entry from the Inorganic Crystal Structure Database, the world’s repository for inorganic crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely availabl…
View article: CSD 1791568: Experimental Crystal Structure Determination
CSD 1791568: Experimental Crystal Structure Determination Open
An entry from the Inorganic Crystal Structure Database, the world’s repository for inorganic crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely availabl…