J. E. Camp
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View article: Scalable synthesis of 3-O functionalized deoxyribonolactones from biorenewable levoglucosenone
Scalable synthesis of 3-O functionalized deoxyribonolactones from biorenewable levoglucosenone Open
A scalable and chromatography-free synthesis of 3-O functionalized deoxyribonolactones from biorenewable levoglucosenone (LGO) is presented. This study enhances the synthesis of the previously reported 2-deoxy-D-ribonolactone by employing …
View article: Oxa-Michael-initiated cascade reactions of levoglucosenone
Oxa-Michael-initiated cascade reactions of levoglucosenone Open
The reactions of aromatic aldehydes and levoglucosenone promoted by methoxide gives bridged α,β-unsaturated ketones, formed by a series of oxa-Michael-initiated cascade reactions in yields of up to 91% (14 examples). A complex series of eq…
View article: Levoglucosenone: Bio-Based Platform for Drug Discovery
Levoglucosenone: Bio-Based Platform for Drug Discovery Open
Levoglucosone (LGO) is a bio-privileged molecule that can be produced on scale from waste biomass. This chiral building block has been converted via well-established chemical processes into previously difficult-to-synthesize building block…
View article: Technoeconomic Assessment of Organic Halide Based Gold Recovery from Waste Electronic and Electrical Equipment
Technoeconomic Assessment of Organic Halide Based Gold Recovery from Waste Electronic and Electrical Equipment Open
Waste Electronic and Electrical Equipment (WEEE) is one of the fastest growing waste streams worldwide, with significant economic value due to the precious metals contained within. Currently, only a small share of the total globally produc…
View article: Synthesis of 2,4-Disubstituted Imidazoles via Nucleophilic Catalysis
Synthesis of 2,4-Disubstituted Imidazoles via Nucleophilic Catalysis Open
A convergent, microwave-assisted protocol for the synthesis of disubstituted NH-imidazoles via nucleophilic catalysis is described. The substituted imidazoles are accessed via the intramolecular addition of a variety of amidoxime substrate…
View article: Correction: Cyrene™ is a green alternative to DMSO as a solvent for antibacterial drug discovery against ESKAPE pathogens
Correction: Cyrene™ is a green alternative to DMSO as a solvent for antibacterial drug discovery against ESKAPE pathogens Open
Correction for ‘Cyrene™ is a green alternative to DMSO as a solvent for antibacterial drug discovery against ESKAPE pathogens’ by Jason E. Camp et al., RSC Med. Chem., 2020, 11, 111–117.
View article: Recent advances in the synthesis of imidazoles
Recent advances in the synthesis of imidazoles Open
The review highlights the recent advances (2018-present) in the regiocontrolled synthesis of substituted imidazoles.
View article: Cyrene™ is a green alternative to DMSO as a solvent for antibacterial drug discovery against ESKAPE pathogens
Cyrene™ is a green alternative to DMSO as a solvent for antibacterial drug discovery against ESKAPE pathogens Open
We describe the evaluation of Cyrene™ as an alternative to DMSO as a vehicle for antibacterial susceptibility testing.
View article: Synthesis of amides from acid chlorides and amines in the bio-based solvent Cyrene™
Synthesis of amides from acid chlorides and amines in the bio-based solvent Cyrene™ Open
Cyrene™ as a bio-alternative dipolar aprotic solvent: a waste minimizing and molar efficient protocol for the synthesis of amides from acid chlorides and primary amines in the bio-available solvent Cyrene™ is disclosed.
View article: Dehydrative Cross-Coupling of 1-Phenylethanol Catalysed by Palladium Nanoparticles Formed in situ Under Acidic Conditions
Dehydrative Cross-Coupling of 1-Phenylethanol Catalysed by Palladium Nanoparticles Formed in situ Under Acidic Conditions Open
A dehydrative cross-coupling of 1-phenylethanol catalysed by sugar derived, in situ formed palladium(0) nanoparticles under acidic conditions is realised. The acidic conditions allow for use of alcohols as a feedstock in metal-mediated cou…
View article: Synthesis of ureas in the bio-alternative solvent Cyrene
Synthesis of ureas in the bio-alternative solvent Cyrene Open
The bio-alternative solvent Cyrene was shown to be an alternative to toxic oil-derived solvents for the synthesis of ureas.
View article: Charge-transfer dynamics at the dye–semiconductor interface of photocathodes for solar energy applications
Charge-transfer dynamics at the dye–semiconductor interface of photocathodes for solar energy applications Open
This article describes a comparison between the photophysical properties of two charge-transfer dyes adsorbed onto NiO via two different binding moieties. Transient spectroscopy measurements suggest that the structure of the anchoring grou…
View article: Exploring the Reactivity of 2-Trichloromethylbenzoxazoles for Access to Substituted Benzoxazoles
Exploring the Reactivity of 2-Trichloromethylbenzoxazoles for Access to Substituted Benzoxazoles Open
The reactivity of 2-trichloromethylbenzoxazoles toward various nucleophiles, under metal-free or iron-catalyzed conditions, for the synthesis of substituted benzoxazoles is described. These methods allow for selective substitution at eithe…
View article: Use of Monosaccharides in Metal-Catalyzed Coupling Reactions
Use of Monosaccharides in Metal-Catalyzed Coupling Reactions Open
The addition of monosaccharides to metal-catalyzed coupling reactions can be beneficial in terms of decreasing the time required, chemical waste products and overall cost of the process. Monosaccharides are used in a number of different wa…
View article: Auto‐Tandem Catalysis: Activation of Multiple, Mechanistically Distinct Process by a Single Catalyst
Auto‐Tandem Catalysis: Activation of Multiple, Mechanistically Distinct Process by a Single Catalyst Open
Auto‐tandem catalysis (ATC) is a powerful method for the synthesis of heterocycles and carbocycles as well as acyclic compounds. The process is defined as a single reagent catalysing multiple, mechanistically distinct processes of a chemic…
View article: CCDC 1503143: Experimental Crystal Structure Determination
CCDC 1503143: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …