Lorena Capdevila
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View article: Interphasic Separation of cis/trans Perylene-Based Nanographene Isomers Driven by Selective Encapsulation in a Supramolecular Cage
Interphasic Separation of cis/trans Perylene-Based Nanographene Isomers Driven by Selective Encapsulation in a Supramolecular Cage Open
The present work describes a supramolecular strategy for the molecular recognition and selective separation of extended PAHs and NGs from isomeric mixtures. This approach consists of a biphasic protocol featuring...
View article: Shortcut to Highly Fluorescent Perylene Derivatives: From Fluoranthene Fissure‐Coupling to Late‐Stage Aromatic Extension
Shortcut to Highly Fluorescent Perylene Derivatives: From Fluoranthene Fissure‐Coupling to Late‐Stage Aromatic Extension Open
Access to extended perylene‐based nanographenes (NGs) is severely limited and involves tedious multi‐step synthetic procedures. Here a two‐step synthesis shortcut to highly soluble, bent, and extended perylene‐based NGs from a nonperylene …
View article: Direct 2,2,2‐Trifluoro and 2,2‐Difluoroethoxylation of a Model Macrocyclic Ar−H Substrate via Ni‐Catalysis
Direct 2,2,2‐Trifluoro and 2,2‐Difluoroethoxylation of a Model Macrocyclic Ar−H Substrate via Ni‐Catalysis Open
Herein, we describe the trifluoro‐ and difluoroethoxylation of C(sp 2 )‐H bonds using nickel(II) complexes incorporating a model macrocyclic arene substrate. Due to the coordinative properties of the macrocyclic substrate, we were able to …
View article: CCDC 2285384: Experimental Crystal Structure Determination
CCDC 2285384: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2285382: Experimental Crystal Structure Determination
CCDC 2285382: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2285383: Experimental Crystal Structure Determination
CCDC 2285383: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: Luminescent Chiral Furanol‐PAHs via Straightforward Ni‐Catalysed C<sub>sp2</sub>−F Functionalization: Mechanistic Insights into the Scholl Reaction
Luminescent Chiral Furanol‐PAHs via Straightforward Ni‐Catalysed C<sub>sp2</sub>−F Functionalization: Mechanistic Insights into the Scholl Reaction Open
Here we report the stepwise synthesis of new nanographenes (NGs) and polycyclic aromatic hydrocarbons (PAHs) obtained via Scholl ring fusion applied at aromatic homologation compounds, which are obtained through one‐step Ni‐catalysed C sp2…
View article: CCDC 2097543: Experimental Crystal Structure Determination
CCDC 2097543: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2097546: Experimental Crystal Structure Determination
CCDC 2097546: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: C<sub>sp2</sub>–H Amination Reactions Mediated by Metastable Pseudo-<i>O</i><sub><i>h</i></sub>Masked Aryl-Co<sup>III</sup>-nitrene Species
C<sub>sp2</sub>–H Amination Reactions Mediated by Metastable Pseudo-<i>O</i><sub><i>h</i></sub>Masked Aryl-Co<sup>III</sup>-nitrene Species Open
Cobalt-catalyzed C-H amination via M-nitrenoid species is spiking the interest of the research community. Understanding this process at a molecular level is a challenging task, and here we report a well-defined macrocyclic system featuring…
View article: CCDC 2097542: Experimental Crystal Structure Determination
CCDC 2097542: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2097544: Experimental Crystal Structure Determination
CCDC 2097544: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2097545: Experimental Crystal Structure Determination
CCDC 2097545: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2144669: Experimental Crystal Structure Determination
CCDC 2144669: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: Nickel‐Catalyzed C<sub>sp2</sub>−OMe Functionalization for Chemoselective Aromatic Homologation En Route to Nanographenes
Nickel‐Catalyzed C<sub>sp2</sub>−OMe Functionalization for Chemoselective Aromatic Homologation En Route to Nanographenes Open
A Ni‐catalyzed C sp2 −OMe ortho ‐functionalization methodology to form chemoselectively alkyne monoannulation or aromatic homologation products is reported as a novel protocol towards the valorisation of substrates containing C sp2 −OMe un…
View article: CCDC 1891021: Experimental Crystal Structure Determination
CCDC 1891021: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: Silver(I)-Catalyzed C–X, C–C, C–N, and C–O Cross-Couplings Using Aminoquinoline Directing Group via Elusive Aryl-Ag(III) Species
Silver(I)-Catalyzed C–X, C–C, C–N, and C–O Cross-Couplings Using Aminoquinoline Directing Group via Elusive Aryl-Ag(III) Species Open
Cross-coupling transformations are a powerful tool in organic synthesis. It is known that this kind of transformation undergoes 2- electron redox processes, and, for this reason, silver has been nearly forgotten as catalyst for cross-coupl…