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View article: <i>Pydidas</i>: a tool for automated X-ray diffraction data analysis
<i>Pydidas</i>: a tool for automated X-ray diffraction data analysis Open
The processing and analysis of X-ray diffraction (XRD) data at synchrotrons is often left to the user groups, which limits the user base to groups with a background in analyzing XRD data. Pydidas is a new Python package for processing XRD …
View article: Fast Degradation of Solid Electrolyte in Initial Cycling Processes, Tracked in 3D by Synchrotron X-ray Computed Tomography
Fast Degradation of Solid Electrolyte in Initial Cycling Processes, Tracked in 3D by Synchrotron X-ray Computed Tomography Open
Solid-state lithium batteries are developing rapidly as a promising next-generation battery, while challenges still persist in understanding their degradation processes during cycling due to the difficulties in characterization. In this st…
View article: Dynamic Evolution of the Transcrustal Plumbing System in Large Igneous Provinces: Geochemical and Microstructural Insights from Glomerocrysts and Melt Inclusions
Dynamic Evolution of the Transcrustal Plumbing System in Large Igneous Provinces: Geochemical and Microstructural Insights from Glomerocrysts and Melt Inclusions Open
The nature of the magma plumbing system of Large Igneous Provinces is still poorly understood. Among these exceptional magmatic events from Earth's past, the end-Triassic Central Atlantic Magmatic Province (CAMP) and the end-Cretaceous Dec…
View article: Multi-modal investigation of the bone micro- and ultrastructure, and elemental distribution in the presence of Mg-xGd screws at mid-term healing stages
Multi-modal investigation of the bone micro- and ultrastructure, and elemental distribution in the presence of Mg-xGd screws at mid-term healing stages Open
Magnesium (Mg) - based alloys are becoming attractive materials for medical applications as temporary bone implants for support of fracture healing, e.g. as a suture anchor. Due to their mechanical properties and biocompatibility, they may…
View article: The transcrustal plumbing system of Large Igneous Provinces: Insights from glomerocrysts and melt inclusions
The transcrustal plumbing system of Large Igneous Provinces: Insights from glomerocrysts and melt inclusions Open
The magma plumbing system throughout the entire transcrustal section of Large Igneous Provinces (LIPs) is still poorly understood. Among the most voluminous LIPs, the Central Atlantic Magmatic Province (CAMP [1], ca. 201 Ma) and the Deccan…
View article: Hard x-ray nanotomography at the P05 imaging beamline at PETRA III
Hard x-ray nanotomography at the P05 imaging beamline at PETRA III Open
Hard X-ray nanotomography is a commonly used tool in many research areas such as material science, biology and medicine. The nanotomography station at the P05 imaging beamline at PETRA III at DESY is operated by the Helmholtz-Zentrum Hereo…
View article: Application of X‑ray Microcomputed Tomography for the Static and Dynamic Characterization of the Microstructure of Oleofoams
Application of X‑ray Microcomputed Tomography for the Static and Dynamic Characterization of the Microstructure of Oleofoams Open
Raw, greyscale image stacks collected during a X-Ray tomography analysis on cocoa butter-based oleofoams. The dataset is divided into three subsets: aeration, storage and heating, which contain samples that have been aerated for different …
View article: Application of X‑ray Microcomputed Tomography for the Static and Dynamic Characterization of the Microstructure of Oleofoams
Application of X‑ray Microcomputed Tomography for the Static and Dynamic Characterization of the Microstructure of Oleofoams Open
Raw, greyscale image stacks collected during a X-Ray tomography analysis on cocoa butter-based oleofoams. The dataset is divided into three subsets: aeration, storage and heating, which contain samples that have been aerated for different …
View article: Application of X-ray Microcomputed Tomography for the Static and Dynamic Characterization of the Microstructure of Oleofoams
Application of X-ray Microcomputed Tomography for the Static and Dynamic Characterization of the Microstructure of Oleofoams Open
Oleofoams are a novel, versatile, and biocompatible soft material that finds application in drug, cosmetic or nutraceuticals delivery. However, due to their temperature-sensitive and opaque nature, the characterization of oleofoams' micros…
View article: High-throughput micro and nano-tomography
High-throughput micro and nano-tomography Open
We report about multiscale tomography with high throughput at the Diamond beamline I13L. The beamline has the purpose of multi-scale and operando imaging and consists of two independent branchlines operating in real and reciprocal space. T…
View article: The Effect of Chemistry and 3D Microstructural Architecture on Corrosion of Biodegradable Mg–Ca–Zn Alloys
The Effect of Chemistry and 3D Microstructural Architecture on Corrosion of Biodegradable Mg–Ca–Zn Alloys Open
The development of biodegradable Mg–Ca–Zn alloys strongly relies on the understanding of the varying 3D microstructural architectures by means of high‐density‐resolution imaging, such as synchrotron radiation–based X‐ray microtomography (S…
View article: 3D analysis of enamel demineralisation in human dental caries using high-resolution, large field of view synchrotron X-ray micro-computed tomography
3D analysis of enamel demineralisation in human dental caries using high-resolution, large field of view synchrotron X-ray micro-computed tomography Open
We report major advances in the analysis of synchrotron 3D datasets acquired from human healthy and carious dental enamel. Synchrotron tomographic data for three human carious samples and a non-carious reference tooth sample were collected…
View article: Functional and multiscale 3D structural investigation of brain tissue through correlative<i>in vivo</i>physiology, synchrotron micro-tomography and volume electron microscopy
Functional and multiscale 3D structural investigation of brain tissue through correlative<i>in vivo</i>physiology, synchrotron micro-tomography and volume electron microscopy Open
Attributing in vivo neurophysiology to the brains’ ultrastructure requires a large field of view containing contextual anatomy. Electron microscopy (EM) is the gold standard technique to identify ultrastructure, yet acquiring volumes conta…
View article: 4D In-Situ Microscopy of Aerosol Filtration in a Wall Flow Filter
4D In-Situ Microscopy of Aerosol Filtration in a Wall Flow Filter Open
The transient nature of the internal pore structure of particulate wall flow filters, caused by the continuous deposition of particulate matter, makes studying their flow and filtration characteristics challenging. In this article we prese…
View article: 4D Bragg Edge Tomography of Directional Ice Templated Graphite Electrodes
4D Bragg Edge Tomography of Directional Ice Templated Graphite Electrodes Open
Bragg edge tomography was carried out on novel, ultra-thick, directional ice templated graphite electrodes for Li-ion battery cells to visualise the distribution of graphite and stable lithiation phases, namely LiC12 and LiC6. The four-dim…
View article: Hard X-ray nano-holotomography with a Fresnel zone plate
Hard X-ray nano-holotomography with a Fresnel zone plate Open
X-ray phase contrast nanotomography enables imaging of a wide range of samples with high spatial resolution in 3D. Near-field holography, as one of the major phase contrast techniques, is often implemented using X-ray optics such as Kirkpa…
View article: Following the effect of braid architecture on performance and damage of carbon fibre/epoxy composite tubes during torsional straining
Following the effect of braid architecture on performance and damage of carbon fibre/epoxy composite tubes during torsional straining Open
The torsional performance of bi-axially braided carbon fibre reinforced polymer (CFRP) tubes as a function of braid architecture is investigated. It is found that for a given braid pattern, the 45° braided CFRP tubes have higher shear modu…
View article: Pushing the temporal resolution in absorption and Zernike phase contrast nanotomography: enabling fast <i>in situ</i> experiments
Pushing the temporal resolution in absorption and Zernike phase contrast nanotomography: enabling fast <i>in situ</i> experiments Open
Hard X-ray nanotomography enables 3D investigations of a wide range of samples with high resolution (<100 nm) with both synchrotron-based and laboratory-based setups. However, the advantage of synchrotron-based setups is the high flux, ena…
View article: Environmentally induced crack (EIC) initiation, propagation, and failure: A 3D in-situ time-lapse study of AA5083 H131
Environmentally induced crack (EIC) initiation, propagation, and failure: A 3D in-situ time-lapse study of AA5083 H131 Open
Environment Induced Cracking (EIC) has been observed in three dimensions (3D) at high spatial and temporal resolution for AA5083 H131 alloy using in situ synchrotron X-ray CT. The initiation of EIC cracks occurred in humid air at ∼0.5σy an…
View article: The Diamond I13 full-field transmission X-ray microscope: a Zernike phase-contrast setup for material sciences
The Diamond I13 full-field transmission X-ray microscope: a Zernike phase-contrast setup for material sciences Open
The I13 transmission X-ray microscope at Diamond Light Source (DLS) has been designed to cover a broad range of energies and field of views. The beamline operates on an undulator source, and a multilayer monochromator can be used to work a…
View article: Fast Multi-scale imaging using the Beamline I13L at the Diamond Light Source
Fast Multi-scale imaging using the Beamline I13L at the Diamond Light Source Open
The DIAMOND beamline I13L is dedicated to multi-scale and multi-modal imaging in real and reciprocal space. The beamline consists of two independently operating experimental stations, located at a distance of more than 200 m from the sourc…
View article: Development of synchrotron pink beam x-ray grating interferometer at the Diamond Light source I13-2 beamline
Development of synchrotron pink beam x-ray grating interferometer at the Diamond Light source I13-2 beamline Open
X-ray Grating Talbot Interferometer (XGTI) is already routinely used for quantitative phase contrast imaging of soft tissue samples. XGTI can be realized using various measurement techniques, depending on the X-ray source used, the require…