Yangjie Wu
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View article: Visible‐Light‐Induced Radical Cyclization of Unactivated Olefins with Perfluoroalkyl Iodides to Access Perfluoroalkylated <i>Ortho</i>‐Diazaheterocyclic Compounds
Visible‐Light‐Induced Radical Cyclization of Unactivated Olefins with Perfluoroalkyl Iodides to Access Perfluoroalkylated <i>Ortho</i>‐Diazaheterocyclic Compounds Open
An efficient visible‐light‐driven strategy for the radical perfluoroalkylation/tandem cyclization of unactivated alkenes with perfluoroalkyl iodides (IR f ) has been developed, enabling efficient synthesis of perfluoroalkylated heterocycli…
View article: The Rise of Green Solvents: Application and Efficiency of Deep Eutectic Solvents in the Extraction of Flavonoids
The Rise of Green Solvents: Application and Efficiency of Deep Eutectic Solvents in the Extraction of Flavonoids Open
Deep eutectic solvents (DESs) provide a sustainable and effective way to extract flavonoids from herbal medicines, which are known for their notable antioxidant effects. Traditional extraction approaches are often costly and utilize harmfu…
View article: Rh(III)‐Catalyzed Cascade [3 + 3] Spiroannulation of <i>N</i>‐Acyl Ketimines with Iodonium Ylides: Access to Spiro‐<i>N,O</i>‐Ketals
Rh(III)‐Catalyzed Cascade [3 + 3] Spiroannulation of <i>N</i>‐Acyl Ketimines with Iodonium Ylides: Access to Spiro‐<i>N,O</i>‐Ketals Open
A Rh(III)‐catalyzed cascade CH activation/[3 + 3]spiroannulation of 3‐hydroxy‐3‐arylisoindolin‐1‐ones with iodonium ylides has been developed. The method facilitates the efficient and selective construction of spirocyclic compounds in a o…
View article: Analysis of serum NLR combined with intraoperative margin condition to predict the prognosis of cervical HSIL patients undergoing LEEP surgery
Analysis of serum NLR combined with intraoperative margin condition to predict the prognosis of cervical HSIL patients undergoing LEEP surgery Open
Objective This study analyzed the prognosis of patients with high-grade squamous intraepithelial lesion (HSIL) after loop electrosurgical excision procedure (LEEP) and elucidated the predictive value of neutrophil-to-lymphocyte ratio (NLR)…
View article: Stability in Composite Bearing Structures within Room-and-Pillar Goafs under Repeated Mining
Stability in Composite Bearing Structures within Room-and-Pillar Goafs under Repeated Mining Open
During repeated mining of shallow and closely spaced coal seams, the failure of coal pillars within the upper goaf can induce dynamic hazards—such as shield jamming, support collapse, and roof fall—at the lower fully mechanized working fac…
View article: Electrochemical α-C(sp3)–H/N–H Cross-Coupling of Isochromans and Azoles
Electrochemical α-C(sp3)–H/N–H Cross-Coupling of Isochromans and Azoles Open
Isochroman and azole moieties are both present in a wide variety of biologically active molecules. Their efficient combination under mild reaction conditions is beneficial for obtaining small-molecule drug candidates. In this paper, we des…
View article: Photocatalytic Regioselective Tandem Cyclization Protocol to Trifluoromethylated Pyrrolidones
Photocatalytic Regioselective Tandem Cyclization Protocol to Trifluoromethylated Pyrrolidones Open
A new environmentally friendly and efficient strategy for preparing trifluoromethylated pyrrolidones has been developed. The process involves using visible light to induce radical cyclization of 1,5‐dienes with CF 3 SO 2 Na, resulting in e…
View article: Nano‐Multiactive Sites Pd/PdO/CuO/PdCu<sub>3</sub> Formed In Situ on the Surface Hetero‐Organometallic Pd(II)/Cu(II) Nanosheet: Investigation on the Formation of Active Sites, Synergistic, and Catalytic Activity
Nano‐Multiactive Sites Pd/PdO/CuO/PdCu<sub>3</sub> Formed In Situ on the Surface Hetero‐Organometallic Pd(II)/Cu(II) Nanosheet: Investigation on the Formation of Active Sites, Synergistic, and Catalytic Activity Open
Exploring the relationship between the structure of active site and the activity in molecular level and investigating the reason for deactivation are extremely important in designing the highly active catalyst. In this paper, new self‐asse…
View article: Enantioselective de novo construction of 3‑oxindoles via organocatalyzed formal [3 + 2] annulation from simple arylamines
Enantioselective de novo construction of 3‑oxindoles via organocatalyzed formal [3 + 2] annulation from simple arylamines Open
The de novo construction of enantioenriched 3-hydroxyindolenines and 3-oxindoles from easily available starting materials has been highly desired. Herein, an enantioselectively intermolecular direct [3 + 2] annulation of aryl amine with 2,…
View article: Synthesis of 1,4-oxathiins via [3+3] annulation of pyridinium 1,4-zwitterionic thiolates with iodonium ylides
Synthesis of 1,4-oxathiins via [3+3] annulation of pyridinium 1,4-zwitterionic thiolates with iodonium ylides Open
A straightforward and valuable approach for the synthesis of 1,4-oxathiins has been developed via [3 + 3] annulation of pyridinium 1,4-zwitterionic thiolates with iodonium ylides. C–S and C–O bonds were formed in one pot manner in this t…
View article: Visual Perception and Multimodal Control: A Novel Approach to Designing an Intelligent Badminton Serving Device
Visual Perception and Multimodal Control: A Novel Approach to Designing an Intelligent Badminton Serving Device Open
Addressing the current issue of limited control methods for badminton serving devices, this paper proposes a vision-based multimodal control system and method for badminton serving. The system integrates computer vision recognition technol…
View article: Rhodium(III)‐Catalyzed C7‐Spiroannulation of Indolines with Maleimides: Facile Access to Aza‐Spiromulticycles
Rhodium(III)‐Catalyzed C7‐Spiroannulation of Indolines with Maleimides: Facile Access to Aza‐Spiromulticycles Open
Herein, we report a chemo‐ and regioselective Rh‐catalyzed redox C7‐spiroannulation reaction of N ‐benzo[ d ]imidazole indolines with maleimides, resulting in a series of N ‐benzo[ d ]imidazole indoline fused azaspirocycles in up to 92% yi…
View article: CCDC 2242954: Experimental Crystal Structure Determination
CCDC 2242954: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: Visible‐Light‐Induced Multicomponent Reaction of Aromatic Aldehydes, Amines and Sodium Difluoromethanesulfinate: Synthesis of CF<sub>2</sub>H‐Substituted Secondary Amines
Visible‐Light‐Induced Multicomponent Reaction of Aromatic Aldehydes, Amines and Sodium Difluoromethanesulfinate: Synthesis of CF<sub>2</sub>H‐Substituted Secondary Amines Open
A visible‐light induced multicomponent reaction of aromatic aldehydes, amines and sodium difluoromethanesulfinate for the synthesis of fluorinated secondary amines has been investigated. The protocol affords a convenient pathway for the in…
View article: Vinylene Carbonate as Synthon in Transition Metal‐Catalyzed C−H Bond Activation/Annulation Reactions
Vinylene Carbonate as Synthon in Transition Metal‐Catalyzed C−H Bond Activation/Annulation Reactions Open
Recently, vinylene carbonate has been developed as a powerful synthon in transition metal‐catalyzed C−H bond activation/cyclization reactions. This review introduces recent progress in the use of vinylene carbonate as a reactant, by analyz…
View article: CCDC 2163249: Experimental Crystal Structure Determination
CCDC 2163249: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2242953: Experimental Crystal Structure Determination
CCDC 2242953: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: De novo construction of chiral 3‑oxindoles via organocatalyzed enantioselective ortho-Friedel-Crafts addition/novel [1,2]-ester migration
De novo construction of chiral 3‑oxindoles via organocatalyzed enantioselective ortho-Friedel-Crafts addition/novel [1,2]-ester migration Open
The de novo construction of chiral 3-hydroxyindolenines and 3-oxindoles from easily available starting materials has been highly desired. Meanwhile, the intermolecular enantioselective ortho -C-H addition to ketone carbonyl remains a long-…
View article: CCDC 2208031: Experimental Crystal Structure Determination
CCDC 2208031: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2211526: Experimental Crystal Structure Determination
CCDC 2211526: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2211522: Experimental Crystal Structure Determination
CCDC 2211522: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2211523: Experimental Crystal Structure Determination
CCDC 2211523: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: Front Cover Picture: Rhodium(III)‐Catalyzed Divergent C−H Functionalization of <i>N</i>‐Aryl Amidines with Iodonium Ylides: Access to Carbazolones and Zwitterionic Salts (Adv. Synth. Catal. 11/2023)
Front Cover Picture: Rhodium(III)‐Catalyzed Divergent C−H Functionalization of <i>N</i>‐Aryl Amidines with Iodonium Ylides: Access to Carbazolones and Zwitterionic Salts (Adv. Synth. Catal. 11/2023) Open
The cover design shows a Chinese fairy tale “Carp jump over the dragon gate”. There was a Dragon Gate on the Yellow River. Carps could jump over it and turn into dragons, which means that everyone should conquer some difficulty before succ…