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View article: Synthesis of α‐Nitroketones through Electrochemical Olefin Oxidation–Nitration
Synthesis of α‐Nitroketones through Electrochemical Olefin Oxidation–Nitration Open
Comprehensive Summary Herein, we report an environmentally friendly electrochemical method for the synthesis of α‐nitroketones from olefins. In this approach, Fe(NO 3 ) 3 ·9H 2 O and trace amounts of H 2 O in the system serve as nitrogen a…
View article: CCDC 2092639: Experimental Crystal Structure Determination
CCDC 2092639: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: Electrochemical benzylicic C–H carbonylation
Electrochemical benzylicic C–H carbonylation Open
This review systematically summarizes recent advances (2019–2025) in electrochemical benzylicic C–H oxidation for the synthesis of benzylic ketones/aldehydes, emphasizing sustainable methodologies. The article critically evaluates both dir…
View article: Multi-component reactions via copper(I) difluorocarbene as carbonyl source for constructing α—aminoamide derivatives
Multi-component reactions via copper(I) difluorocarbene as carbonyl source for constructing α—aminoamide derivatives Open
Difluorocarbene, an important reactive intermediate in organic synthesis, exhibits intriguing properties and synthetic versatility. However, great challenges in modulating reaction pathways limit its widespread application in synthetic che…
View article: Electrochemical Conversion of Low-Concentration CO<sub>2</sub> Promoted by a Guanidine Polymer
Electrochemical Conversion of Low-Concentration CO<sub>2</sub> Promoted by a Guanidine Polymer Open
In situ electrocatalytic conversion of low-concentration carbon dioxide (CO2) from anaerobic fermentation gas (AFG) into high-value chemical products can effectively mitigate the costs associated with carbon capture, enrichment, and transf…
View article: Phosphorus‐Doped Single Atom Copper Catalyst as a Redox Mediator in the Cathodic Reduction of Quinazolinones
Phosphorus‐Doped Single Atom Copper Catalyst as a Redox Mediator in the Cathodic Reduction of Quinazolinones Open
The use of clean electric energy to activate inert compounds has garnered significant attention. Homogeneous redox mediators (RMs) in organic electrosynthesis are effective platforms for this purpose. However, understanding the RM's electr…
View article: Phosphorus‐Doped Single Atom Copper Catalyst as a Redox Mediator in the Cathodic Reduction of Quinazolinones
Phosphorus‐Doped Single Atom Copper Catalyst as a Redox Mediator in the Cathodic Reduction of Quinazolinones Open
The use of clean electric energy to activate inert compounds has garnered significant attention. Homogeneous redox mediators (RMs) in organic electrosynthesis are effective platforms for this purpose. However, understanding the RM's electr…
View article: Design Concepts and Synthesis Strategies for Porous Organic Polymers‐Based Catalysts: Targeting the in‐situ Conversion of Low‐concentration CO<sub>2</sub> into Value‐added Chemicals
Design Concepts and Synthesis Strategies for Porous Organic Polymers‐Based Catalysts: Targeting the in‐situ Conversion of Low‐concentration CO<sub>2</sub> into Value‐added Chemicals Open
Porous organic polymers (POPs)‐based catalysts have emerged as promising materials for the conversion of low‐concentration CO 2 into valuable chemicals, leveraging their high specific surface area, designability, multifunctionality, except…
View article: Direct conversion of waste CO <sub>2</sub> over porous polymer catalysts
Direct conversion of waste CO <sub>2</sub> over porous polymer catalysts Open
In this review, the most recent advances in the design and synthesis of porous polymer catalysts for the conversion of waste CO 2 are summarized. The main highlight is the activation and enrichment mechanism of CO 2 in porous polymer catal…
View article: A Mn–Rh dual single-atom catalyst for inducing C–C cleavage: relay catalysis reversing chemoselectivity in C–H oxidation
A Mn–Rh dual single-atom catalyst for inducing C–C cleavage: relay catalysis reversing chemoselectivity in C–H oxidation Open
We developed a Mn, Rh DSAC (Mn 1 –Rh 1 @O-TiC) with high efficiency for cumene oxidation, enabling effective AP production. This work offers key insights into designing catalytic systems for organic tandem reactions from an inorganic chemi…
View article: Electrochemical Esterification Reaction of Alkyne Aldehyde with Alcohols Mediated by Carbene and Iodine
Electrochemical Esterification Reaction of Alkyne Aldehyde with Alcohols Mediated by Carbene and Iodine Open
A new type of alkyne esterification was developed under electrochemical conditions using alkyne aldehydes and alcohol compounds as starting materials and carbene and iodine as mediators. Through this method, external oxidants and transitio…
View article: Visible‐Light‐Mediated Vinyl‐Thiophosphate Formation <i>Via</i> Three‐Component Denitrative Cross‐Coupling Reaction
Visible‐Light‐Mediated Vinyl‐Thiophosphate Formation <i>Via</i> Three‐Component Denitrative Cross‐Coupling Reaction Open
A three‐component denitrative cross‐coupling reaction mediated by visible light has been developed. Various 2‐arylvinyl thiophosphate compounds were synthesized with moderate‐to‐good yields using cheap, nontoxic, nonvolatile, and non‐hygro…
View article: Electrochemically Promoted Skeleton Transformation of 2,1‐Benzisoxazoles to Alkyl Sulfones
Electrochemically Promoted Skeleton Transformation of 2,1‐Benzisoxazoles to Alkyl Sulfones Open
This study developed an electrochemically promoted skeleton transformation reaction of 2,1‐benzisoxazoles to synthesize alkyl sulfones. Alkyl sulfones were synthesized in 68–93% yield by using 2,1‐benzisoxazole and sulfonate as substrates,…
View article: Single‐Atom Iron Catalyst as an Advanced Redox Mediator for Anodic Oxidation of Organic Electrosynthesis
Single‐Atom Iron Catalyst as an Advanced Redox Mediator for Anodic Oxidation of Organic Electrosynthesis Open
Homogeneous electrocatalysts can indirect oxidate the high overpotential substrates through single‐electron transfer on the electrode surface, enabling efficient operation of organic electrosynthesis catalytic cycles. However, the problems…
View article: Copper‐Metallized Porous <i>N</i>‐Heterocyclic Carbene Ligand Polymer‐Catalyzed Regio‐ and Stereoselective 1,2‐Carboboration of Alkynes
Copper‐Metallized Porous <i>N</i>‐Heterocyclic Carbene Ligand Polymer‐Catalyzed Regio‐ and Stereoselective 1,2‐Carboboration of Alkynes Open
Alkenylboronates are highly versatile building blocks and valuable reagents in the synthesis of complex molecules. Compared with that of monosubstituted alkenylboronates, the synthesis of multisubstituted alkenylboronates is challenging. T…
View article: Single‐Atom Manganese‐Catalyzed Oxygen Evolution Drives the Electrochemical Oxidation of Silane to Silanol
Single‐Atom Manganese‐Catalyzed Oxygen Evolution Drives the Electrochemical Oxidation of Silane to Silanol Open
The oxygen evolution reaction (OER), characterized by a four‐electron transfer kinetic process, represents a significant bottleneck in improving the efficiency of hydrogen production from water electrolysis. Consequently, extensive researc…
View article: Recent Advances in Electrochemically Mediated Reactions of Diselenides
Recent Advances in Electrochemically Mediated Reactions of Diselenides Open
Organoselenium compounds are crucial molecules that are utilized extensively in diverse fields such as medicine, agriculture, catalysis, and organic materials. The incorporation of selenium atoms into organic molecules holds significant im…
View article: Electrochemical Three‐Component Reaction to Construct <i>N</i>‐(<i>α</i>‐alkoxyalkyl)benzotriazoles
Electrochemical Three‐Component Reaction to Construct <i>N</i>‐(<i>α</i>‐alkoxyalkyl)benzotriazoles Open
N ‐( α ‐alkoxyalkyl)benzotriazoles are of great importance for biochemical and antitumor activity. A feasible protocol has been developed for the synthesis of N ‐( α ‐alkoxyalkyl)benzotriazoles using azoles, aldehydes and alcohols as subst…
View article: CCDC 2268403: Experimental Crystal Structure Determination
CCDC 2268403: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: Electrochemically Mediated Fixation of CO<sub>2</sub>: Synthesis of Functionalized Oxazolidine‐2,4‐Diones by Three‐Component Reactions
Electrochemically Mediated Fixation of CO<sub>2</sub>: Synthesis of Functionalized Oxazolidine‐2,4‐Diones by Three‐Component Reactions Open
Carbon dioxide is a harmful greenhouse gas, as well as a valuable resource. Here, a three‐component cyclization reaction was developed for the synthesis of oxazolidine‐2,4‐diones by immobilizing CO 2 under the electrochemistry and copper c…
View article: Balance of Interests and Dispute Resolution in the Retrofitting of Elevators in Existing Multi-Story Houses in Tianjin
Balance of Interests and Dispute Resolution in the Retrofitting of Elevators in Existing Multi-Story Houses in Tianjin Open
With the aging of China’s population, the retrofitting of elevators in existing multi-story residential buildings has been steadily promoted with the support of the government, but the regulations and policies guiding the retrofitting of e…
View article: Electrochemical Hydrosilylation of Electron‐Withdrawing Alkenes
Electrochemical Hydrosilylation of Electron‐Withdrawing Alkenes Open
In the presence of the Suginome reagent (PhMe 2 Si−Bpin), a large panel of electron‐withdrawing alkenes was successfully converted into the hydrosilylated product in good to excellent yields. This direct electrochemical hydrosilylation doe…
View article: CCDC 2208586: Experimental Crystal Structure Determination
CCDC 2208586: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2109377: Experimental Crystal Structure Determination
CCDC 2109377: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: Transition metal-free catalytic formylation of carbon dioxide and amide with novel poly(ionic liquid)s
Transition metal-free catalytic formylation of carbon dioxide and amide with novel poly(ionic liquid)s Open
Functionalised mesoporous poly(ionic liquid)s are valuable carbon dioxide capture and conversion materials. Here, an imidazole poly(ionic liquid) PIL-s1-HCO3 with a mesoporous structure was formed by the copolymerisation of vinyl-modified …