Peter Gärtner
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View article: Selective Monoreduction of 2,4 Diazido-Dideoxy Hexoses by Hydrogenation over Lindlar Catalyst
Selective Monoreduction of 2,4 Diazido-Dideoxy Hexoses by Hydrogenation over Lindlar Catalyst Open
A novel, mild and site-selective hydrogenation of equatorial azides in diazido hexoses, achieved using Lindlar catalyst, is reported. Optimization studies on l-β-2,4-dideoxy-diazido rhamnoside revealed exclusive reduction of the equatorial…
View article: Development of an Efficient Stereoretentive <i>Para</i> ‐Claisen‐Cope Rearrangement
Development of an Efficient Stereoretentive <i>Para</i> ‐Claisen‐Cope Rearrangement Open
A stereoretentive para ‐Claisen‐Cope rearrangement of chiral aryl‐allyl ethers is reported, achieving near‐perfect chirality transfer thereby furnishing products with exceptional enantiomeric excess (up to > 98% ee ) as single regioisomers…
View article: CCDC 2048363: Experimental Crystal Structure Determination
CCDC 2048363: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2271072: Experimental Crystal Structure Determination
CCDC 2271072: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: Crystal structures of two 1,2,3,4-tetrahydronaphthalenes obtained during efforts towards the total synthesis of elisabethin A
Crystal structures of two 1,2,3,4-tetrahydronaphthalenes obtained during efforts towards the total synthesis of elisabethin A Open
The two substituted 1,2,3,4-tetrahydronaphthalenes, methyl ( R )-3-{(1 R ,4 S )-6-methoxy-4,7-dimethyl-5,8-bis[(triisopropylsilyl)oxy]-1,2,3,4-tetrahydronaphthalen-1-yl}butanoate, C 36 H 66 O 5 Si 2 , ( 2 ), and methyl ( E )-3-{(1 R ,4 S )…
View article: A biomimetic approach for the concise total synthesis of greenwaylactams A–C
A biomimetic approach for the concise total synthesis of greenwaylactams A–C Open
A concise, racemic total synthesis of three sesquiterpenoid alkaloids (greenwaylactams A–C) exhibiting an unprecedented 8-membered benzolactam is disclosed.
View article: Synthesis and conformational analysis of a potentially super-armed glucuronidation donor
Synthesis and conformational analysis of a potentially super-armed glucuronidation donor Open
The concise synthesis of a potentially “super-armed” glucuronidation donor is reported. The α-anomer was crystallized and analyzed by single crystal X-ray diffraction. The pyranose ring was found to be in a twist-boat conformation in the s…
View article: Detection of DHCMT long-term metabolite glucuronides with LC-MSMS as an alternative approach to conventional GC-MSMS analysis
Detection of DHCMT long-term metabolite glucuronides with LC-MSMS as an alternative approach to conventional GC-MSMS analysis Open
Dehydrochloromethyltestosterone (DHCMT) is one of the most detected illicit used anabolic-androgenic steroids in professional sports. Therefore, a fast and accurate analysis of this substance is of great importance for a constructive fight…
View article: Stanozolol‐N‐glucuronide metabolites in human urine samples as suitable targets in terms of routine anti‐doping analysis
Stanozolol‐N‐glucuronide metabolites in human urine samples as suitable targets in terms of routine anti‐doping analysis Open
The exogenous anabolic‐androgenic steroid (AAS) stanozolol stays one of the most detected substances in professional sports. Its detection is a fundamental part of doping analysis, and the analysis of this steroid has been intensively inve…
View article: Synthesis of human long-term metabolites of dehydrochloromethyltestosterone and oxymesterone
Synthesis of human long-term metabolites of dehydrochloromethyltestosterone and oxymesterone Open
We herein report the synthesis of the long-term metabolites "M4" (IUPAC: 4-chloro-17-hydroxymethyl-17-methyl-18-norandrosta-4,13-dien-3-ol) of dehydrochloromethyl-testosterone (DHCMT, Oral Turinabol) and "Oxy M9" (4-hydroxy-17β-hydroxymeth…
View article: Development and validation of a simple online‐SPE method coupled to high‐resolution mass spectrometry for the analysis of stanozolol‐N‐glucuronides in urine samples
Development and validation of a simple online‐SPE method coupled to high‐resolution mass spectrometry for the analysis of stanozolol‐N‐glucuronides in urine samples Open
Stanozolol is still the most commonly used illicit anabolic‐androgenic steroid (AAS) in professional sports. Therefore, accurate and fast analysis and long detection windows are of great interest in the field of antidoping analysis. In thi…
View article: Banshee distribution network benchmark and prototyping platform for hardware‐in‐the‐loop integration of microgrid and device controllers
Banshee distribution network benchmark and prototyping platform for hardware‐in‐the‐loop integration of microgrid and device controllers Open
This article provides a unique benchmark to integrate and systematically evaluate advanced functionalities of microgrid and downstream device controllers. The article describes Banshee, a real‐life power distribution network. It also detai…
View article: CCDC 1586620: Experimental Crystal Structure Determination
CCDC 1586620: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: Synthesis and structural elucidation of a dehydrochloromethyltestosterone metabolite
Synthesis and structural elucidation of a dehydrochloromethyltestosterone metabolite Open
The identity of a human long-term metabolite of the doping agent Oral Turinabol (DHCMT) is secured by the synthesis of all probable stereoisomers.
View article: CCDC 1586619: Experimental Crystal Structure Determination
CCDC 1586619: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 1586622: Experimental Crystal Structure Determination
CCDC 1586622: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 1825768: Experimental Crystal Structure Determination
CCDC 1825768: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 1586621: Experimental Crystal Structure Determination
CCDC 1586621: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 1517327: Experimental Crystal Structure Determination
CCDC 1517327: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: From waste to value – direct utilization of limonene from orange peel in a biocatalytic cascade reaction towards chiral carvolactone
From waste to value – direct utilization of limonene from orange peel in a biocatalytic cascade reaction towards chiral carvolactone Open
We investigated the valorisation of limonene containing waste product orange peel, and performed a biocatalytic cascade for the production of chiral carvolactone solely in water.