Sayad Doobary
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View article: Mechanochemical Synthesis of <i>X</i> ‐Vinylbenziodoxol(on)es and One‐Pot Conversion to Complex Alkenes <sup>**</sup>
Mechanochemical Synthesis of <i>X</i> ‐Vinylbenziodoxol(on)es and One‐Pot Conversion to Complex Alkenes <sup>**</sup> Open
Densely functionalized alkenes are often utilized as excellent tools for further functionalization of molecules. Recent progress in their synthesis includes nucleophilic addition to vinylbenziodoxolones (VBX) and vinylbenziodoxoles (VBO) t…
View article: Mechanochemical one-pot synthesis of complex alkenes
Mechanochemical one-pot synthesis of complex alkenes Open
Densely functionalized alkenes are often utilized as excellent tools for further functionalization of molecules. Recent progress in their synthesis includes nucleophilic addition to vinylbenziodoxolones (VBX) and vinylbenziodoxolones (VBO)…
View article: Mechanochemical one-pot synthesis of complex alkenes
Mechanochemical one-pot synthesis of complex alkenes Open
Densely functionalized alkenes are often utilized as excellent tools for further functionalization of molecules. Recent progress in their synthesis includes nucleophilic addition to vinylbenziodoxolones (VBX) and vinylbenziodoxolones (VBO)…
View article: Correction: Sustainable and scalable one-pot synthesis of diaryliodonium salts
Correction: Sustainable and scalable one-pot synthesis of diaryliodonium salts Open
Correction for ‘Sustainable and scalable one-pot synthesis of diaryliodonium salts’ by Sayad Doobary et al. , Chem. Commun. , 2025, 61 , 5158–5161, https://doi.org/10.1039/D5CC00774G.
View article: Sustainable and scalable one-pot synthesis of diaryliodonium salts
Sustainable and scalable one-pot synthesis of diaryliodonium salts Open
Two one-pot syntheses of diaryliodonium triflates are presented, rendering the production of these electrophilic arylating agents more sustainable.
View article: Nanocellulose: New horizons in organic chemistry and beyond
Nanocellulose: New horizons in organic chemistry and beyond Open
The study of different forms of nanocellulose is a fast-growing field with many advantages. As a biobased polymer, it holds strong promise to replace petrochemical solid supports that need to be phased out. While there are already a pletho…
View article: Diastereodivergent nucleophile–nucleophile alkene chlorofluorination
Diastereodivergent nucleophile–nucleophile alkene chlorofluorination Open
The selective hetero-dihalogenation of alkenes provides useful building blocks for a broad range of chemical applications. Unlike homo-dihalogenation, selective hetero-dihalogenation reactions, especially fluorohalogenation, are underdevel…
View article: Alkene 1,3‐Difluorination via Transient Oxonium Intermediates
Alkene 1,3‐Difluorination via Transient Oxonium Intermediates Open
The 1,3‐difunctionalization of unactivated alkenes is an under‐explored transformation that leads to moieties that are otherwise challenging to prepare. Herein, we report a hypervalent iodine‐mediated 1,3‐difluorination of homoallylic (ary…
View article: Alkene 1,3‐Difluorination via Transient Oxonium Intermediates
Alkene 1,3‐Difluorination via Transient Oxonium Intermediates Open
The 1,3‐difunctionalization of unactivated alkenes is an under‐explored transformation that leads to moieties that are otherwise challenging to prepare. Herein, we report a hypervalent iodine‐mediated 1,3‐difluorination of homoallylic (ary…
View article: Structure-reactivity analysis of novel hypervalent iodine reagents in S-vinylation of thiols
Structure-reactivity analysis of novel hypervalent iodine reagents in S-vinylation of thiols Open
The transition-metal free S -vinylation of thiophenols by vinylbenziodoxolones (VBX) constituted an important step forward in hypervalent iodine-mediated vinylations, highlighting the difference to vinyliodonium salts and that the reaction…
View article: Hypervalent iodine chemistry with a mechanochemical twist
Hypervalent iodine chemistry with a mechanochemical twist Open
An assessment of mechanochemistry's utility with hypervalent iodine reagents highlighted its effectiveness, which showed better selectivity, reaction times and differing reactivity.
View article: 3D Printed Reactionware for Synthetic Electrochemistry with Hydrogen Fluoride Reagents
3D Printed Reactionware for Synthetic Electrochemistry with Hydrogen Fluoride Reagents Open
Electrochemical fluorination reactions of organic compounds frequently employ hydrogen fluoride reagents that are corrosive. The corrosive nature of these reagents necessitates either the construction or purchase of cells that are stable t…
View article: 3D print files for electrochemical reactors
3D print files for electrochemical reactors Open
.stl files for 3D printing electrochemical reactors designed by the LennoxLab
View article: Electrochemical Vicinal Difluorination of Alkenes: Scalable and Amenable to Electron‐Rich Substrates
Electrochemical Vicinal Difluorination of Alkenes: Scalable and Amenable to Electron‐Rich Substrates Open
Fluorinated alkyl groups are important motifs in bioactive compounds, positively influencing pharmacokinetics, potency and conformation. The oxidative difluorination of alkenes represents an important strategy for their preparation, yet cu…
View article: Electrochemical Vicinal Difluorination of Alkenes: Scalable and Amenable to Electron‐Rich Substrates
Electrochemical Vicinal Difluorination of Alkenes: Scalable and Amenable to Electron‐Rich Substrates Open
Fluorinated alkyl groups are important motifs in bioactive compounds, positively influencing pharmacokinetics, potency and conformation. The oxidative difluorination of alkenes represents an important strategy for their preparation, yet cu…
View article: Electrochemical Vicinal Difluorination of Alkenes: Sustainable, Scalable, and Amenable to Electron-rich Substrates
Electrochemical Vicinal Difluorination of Alkenes: Sustainable, Scalable, and Amenable to Electron-rich Substrates Open
Fluorinated alkyl groups are important motifs in bioactive compounds, positively influencing pharmacokinetics, potency and F conformation. The oxidative difluorination of alkenes represents an H important strategy for their preparation, ye…
View article: Electrochemical Vicinal Difluorination of Alkenes: Sustainable, Scalable, and Amenable to Electron-rich Substrates
Electrochemical Vicinal Difluorination of Alkenes: Sustainable, Scalable, and Amenable to Electron-rich Substrates Open
Fluorinated alkyl groups are important motifs in bioactive compounds, positively influencing pharmacokinetics, potency and F conformation. The oxidative difluorination of alkenes represents an H important strategy for their preparation, ye…