Brian W. Skelton
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View article: CCDC 2473785: Experimental Crystal Structure Determination
CCDC 2473785: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: Heterocyclic core modifications in trypanosomacidal 2-[(phenylheteroaryl)ethyl]ureas
Heterocyclic core modifications in trypanosomacidal 2-[(phenylheteroaryl)ethyl]ureas Open
The protozoan parasites Trypanosoma brucei and T. cruzi cause African sleeping sickness and Chagas disease, respectively. SAR for antitrypanosomal 2-[(phenylheteroaryl)ethyl]amides and ureas was expanded, identifying promising oxazoles and…
View article: Heterometallic CuCd and Cu2Zn complexes with o-vanillin and its Schiff base derivative: slow magnetic relaxation and catalytic activity associated with Cu(II) centers
Heterometallic CuCd and Cu2Zn complexes with o-vanillin and its Schiff base derivative: slow magnetic relaxation and catalytic activity associated with Cu(II) centers Open
In this work, two novel heterometallic mixed-ligand mixed-anion complexes [CuIICdIIClL(o-Van)(OAc)]·3H2O (1) and [CuII2ZnIICl2L2(o-Van)(OAc)] (2) were prepared by reacting a fine copper powder and Cd(II) or Zn(II) acetate with ethanol solu…
View article: Halogen-Dependent Diversity and Weak Interactions in the Heterometallic Ni/Cd Complex Solids: Structural and Theoretical Investigation
Halogen-Dependent Diversity and Weak Interactions in the Heterometallic Ni/Cd Complex Solids: Structural and Theoretical Investigation Open
Three novel heterometallic Ni/Cd coordination compounds [Ni(en)3][CdCl4]∙3dmso (1), [Ni(en)2(dmf)2][CdBr4] (2), and [Ni(en)3]2[CdI4](I)2 (3) have been synthesized through the self-assembly process in a one-pot reaction of cadmium oxide, ni…
View article: CCDC 2141773: Experimental Crystal Structure Determination
CCDC 2141773: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2249877: Experimental Crystal Structure Determination
CCDC 2249877: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2280765: Experimental Crystal Structure Determination
CCDC 2280765: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2280763: Experimental Crystal Structure Determination
CCDC 2280763: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2280766: Experimental Crystal Structure Determination
CCDC 2280766: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2249879: Experimental Crystal Structure Determination
CCDC 2249879: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2280764: Experimental Crystal Structure Determination
CCDC 2280764: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2249876: Experimental Crystal Structure Determination
CCDC 2249876: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2249878: Experimental Crystal Structure Determination
CCDC 2249878: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: Inert Transition Metal Ion Complexes in Organic Synthesis: Protection and Activation
Inert Transition Metal Ion Complexes in Organic Synthesis: Protection and Activation Open
Single‐crystal X‐ray diffraction studies for a variety of metal ion complexes of functionalised sarcophagines (sarcophagine=sar=3,6,10,13,16,19‐hexa‐azabicyclo[6.6.6]icosane) have further confirmed not only that the form of the metal ion/s…
View article: Synthesis of R- and S-MDMA via nucleophilic ring-opening of homochiral N-tosylaziridines
Synthesis of R- and S-MDMA via nucleophilic ring-opening of homochiral N-tosylaziridines Open
Homochiral (R)- and (S)-3,4-methylenedioxymethamphetamine (MDMA) were prepared in six steps (each) from the chiral pool precursors d- and l-alanine, respectively. The key step, copper-catalysed regioselective ring-opening of an N-tosylazir…
View article: Iminophenol as a ligand or cation in cobalt(II and II,III) complexes: synthetic approaches, spectral and structural studies
Iminophenol as a ligand or cation in cobalt(II and II,III) complexes: synthetic approaches, spectral and structural studies Open
New complexes [H2L]2CoCl4 (І) and [CoІІCоІІІCl2L3]H2O (ІІ), where HL is a condensation product of o-vanillin and methylamine, were synthesized and characterized by IR, UV/Vis spectroscopies, and X-ray structural analysis. For the synthesi…
View article: Synthesis, crystal structure and Hirshfeld surface analysis of the hybrid salt bis(2-methylimidazo[1,5-<i>a</i>]pyridin-2-ium) tetrachloridomanganate(II)
Synthesis, crystal structure and Hirshfeld surface analysis of the hybrid salt bis(2-methylimidazo[1,5-<i>a</i>]pyridin-2-ium) tetrachloridomanganate(II) Open
The 0-D hybrid salt bis(2-methylimidazo[1,5- a ]pyridin-2-ium) tetrachloridomanganate(II), (C 8 H 9 N 2 ) 2 [MnCl 4 ] or [ L ] 2 [MnCl 4 ], consists of discrete L + cations and tetrachloridomanganate(II) anions. The fused heterocyclic ring…
View article: CCDC 2182720: Experimental Crystal Structure Determination
CCDC 2182720: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2195415: Experimental Crystal Structure Determination
CCDC 2195415: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2182719: Experimental Crystal Structure Determination
CCDC 2182719: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2064770: Experimental Crystal Structure Determination
CCDC 2064770: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2070615: Experimental Crystal Structure Determination
CCDC 2070615: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2063851: Experimental Crystal Structure Determination
CCDC 2063851: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2078016: Experimental Crystal Structure Determination
CCDC 2078016: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2111366: Experimental Crystal Structure Determination
CCDC 2111366: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2121985: Experimental Crystal Structure Determination
CCDC 2121985: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2065010: Experimental Crystal Structure Determination
CCDC 2065010: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: CCDC 2116434: Experimental Crystal Structure Determination
CCDC 2116434: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …
View article: o-Nitrophenylacetonitrile Michael additions and cyclocondensations: a novel quinoline synthesis
o-Nitrophenylacetonitrile Michael additions and cyclocondensations: a novel quinoline synthesis Open
Michael additions of o-nitrophenylacetonitrile have been investigated.The adducts are formed diastereoselectively under mild conditions.Higher temperatures result in an unusual annulation involving intramolecular nucleophilic attack of an …
View article: CCDC 2204924: Experimental Crystal Structure Determination
CCDC 2204924: Experimental Crystal Structure Determination Open
An entry from the Cambridge Structural Database, the world’s repository for small molecule crystal structures. The entry contains experimental data from a crystal diffraction study. The deposited dataset for this entry is freely available …